Encapsulated Benefit Agent Purification Without Formaldehyde Scavengers

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Solution Overview

Problem

Encapsulated benefit agents in personal care and fabric care compositions often require scavenger materials to manage residual by-products like formaldehyde, increasing formulation complexity and compatibility issues with raw materials.

Innovation Solution

Developing encapsulated benefit agent delivery compositions with reduced or no scavenger materials, using processes like centrifugation, filtration, and solvent exchange to minimize shell particles and manage by-product levels, thereby maintaining lower formaldehyde levels.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Object-affected harmful factors

If scavenger materials are introduced into the slurry to manage residual formaldehyde, then formaldehyde levels are controlled, but formulation complexity increases and compatibility issues with raw materials arise

Engineering Contradiction:
Improveformaldehyde residuesVSAvoidformulation complexity
Core Design Contradiction:
Object-affected harmful factorsVSDevice complexity

Solution Approach 1:

The patent extracts and removes shell particles containing residual formaldehyde from the encapsulated benefit agent composition through filtration and centrifugation processes. This eliminates the need for scavenger materials by physically removing the source of formaldehyde residues, thereby reducing formulation complexity while maintaining formaldehyde control

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent uses filtration and centrifugation as intermediary processes to separate and remove shell particles from the composition. These intermediary steps act as a mediator between the encapsulation process and the final product, eliminating formaldehyde-containing by-products without requiring chemical scavengers that would increase formulation complexity

Inventive Principle:
Principle #24Intermediary (Mediator)

2Object-affected harmful factors

If scavenger materials are introduced into the slurry to manage residual formaldehyde, then formaldehyde levels are controlled, but compatibility issues with raw materials occur

Engineering Contradiction:
Improveformaldehyde residuesVSAvoidraw material compatibility
Core Design Contradiction:
Object-affected harmful factorsVSAdaptability or versatility

Solution Approach 1:

By extracting and removing shell particles that contain residual formaldehyde through physical separation processes, the patent eliminates the need for scavenger materials. This approach maintains raw material compatibility while effectively controlling formaldehyde levels, as no scavenger materials are introduced that could conflict with other formulation components

Inventive Principle:
Principle #2Taking out (Extraction)

3Productivity

If encapsulation processes are used to improve benefit agent delivery efficiency, then delivery efficiency is improved, but residual formaldehyde and shell particles are generated

Engineering Contradiction:
Improvebenefit agent delivery efficiencyVSAvoidresidual formaldehyde
Core Design Contradiction:
ProductivityVSObject-generated harmful factors

Solution Approach 1:

The patent converts the harmful by-products of encapsulation (shell particles containing formaldehyde) into removable waste materials. Through filtration and centrifugation, these previously harmful by-products are systematically removed, allowing the encapsulation process to maintain its benefit agent delivery efficiency improvements while eliminating the associated formaldehyde residues

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

Solution Approach 2:

The patent discards shell particles containing residual formaldehyde through filtration and centrifugation processes. By separating and removing these harmful by-products from the beneficial encapsulated benefit agents, the process recovers the high-value encapsulated product while discarding the formaldehyde-containing waste, thereby improving delivery efficiency without the formaldehyde penalty

Inventive Principle:
Principle #34Discarding and recovering

4Productivity

If encapsulation processes are used to improve benefit agent delivery efficiency, then delivery efficiency is improved, but formulation complexity increases due to scavenger requirements

Engineering Contradiction:
Improvebenefit agent delivery efficiencyVSAvoidformulation complexity
Core Design Contradiction:
ProductivityVSDevice complexity

Solution Approach 1:

The patent extracts and removes shell particles from the encapsulated benefit agent composition through filtration and centrifugation. This extraction eliminates the need for scavenger materials, thereby maintaining the improved benefit agent delivery efficiency while reducing formulation complexity by removing the scavenger requirement

Inventive Principle:
Principle #2Taking out (Extraction)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The approach results in compositions with enhanced benefit agent delivery efficiency and reduced formaldehyde residues, simplifying formulation and improving compatibility with consumer products.

Implementation Method 1

The continuous centrifuge receives a slurry of encapsulated benefit agents and shell particles and separates the shell particles from the encapsulated benefit agents

Methodology Applied
Scientific EffectCentrifugal separation: Centrifugal Separation

Implementation Method 2

The filtration process removes residual shell particles and by-products from the slurry, reducing formaldehyde levels to less than 100 ppm

Methodology Applied
Scientific EffectFiltration: Filter (physical)

Implementation Method 3

solvent exchange to minimize shell particles and manage by-product levels, thereby maintaining lower formaldehyde levels

Methodology Applied
Scientific EffectSolvent exchange: Liquid-Liquid Extraction

Data Source

PatentUS8974547B2Delivery particle
Publication Date: 2015.03.10 ENCAPSYS LLC
  • US8974547B2 patent drawing
  • US8974547B2 patent drawing

AI summary

The present application relates to encapsulated benefit agents, compositions comprising such encapsulated benefit agents and processes for making and using compositions comprising such encapsulated benefit agents that do not require or require a reduced amount of scavenger materials. Such encapsulated benefit agents, compositions comprising such encapsulated benefit agents are processed such that no or lower levels of scavenger materials are required.