Cylindrically Bent Crystal X-ray Spectrometer

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Solution Overview

Problem

Conventional x-ray spectrometers are complex, expensive, and lack portability, requiring intricate operation and control of multiple components, while they diffract from a single point, leading to inefficiencies due to inconsistencies along the diffractor.

Innovation Solution

A portable x-ray spectrometer apparatus using a hollow cylinder with a defracting element forming a ring on its interior circumference and disks to limit the angle of incidence, allowing energy selection by scanning the entire detector/spectrometer assembly toward or away from the sample, eliminating the need for precise control of multiple components and reducing complexity.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If conventional diffractive detection devices are used, then energy resolution is improved (greater than 1 eV), but device complexity and size increase significantly

Engineering Contradiction:
Improveenergy resolutionVSAvoiddevice complexity
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The invention employs a cylindrically bent crystal instead of a flat crystal. The crystal is curved with a radius of curvature between 0.5 meters and 2 meters, which provides natural focusing of diffracted x-rays in the vertical direction. This curvature eliminates the need for complex focusing optics while maintaining high energy resolution, directly resolving the contradiction between measurement precision and device complexity.

Inventive Principle:
Principle #14Spheroidality (Curvature)

2Measurement precision

If conventional von Hamos spectrometer with multiple components is used, then energy resolution is improved, but ease of operation deteriorates due to intricate control requirements

Engineering Contradiction:
Improveenergy resolutionVSAvoidease of operation
Core Design Contradiction:
Measurement precisionVSEase of operation

Solution Approach 1:

The invention combines the x-ray source, cylindrically bent crystal, and position-sensitive detector into a single integrated spectrometer assembly. This merging of components eliminates the need for separate control mechanisms for each component, reducing operational complexity. The assembly operates as a unified system where the detector is positioned at the focal line of the bent crystal, automatically achieving proper geometric alignment without requiring intricate adjustment procedures.

Inventive Principle:
Principle #5Merging (Combining)

3Measurement precision

If conventional systems with fixed component positions are used, then focusing in vertical direction is achieved, but adaptability to different energy ranges is limited

Engineering Contradiction:
Improvefocusing capabilityVSAvoidenergy range coverage
Core Design Contradiction:
Measurement precisionVSAdaptability or versatility

Solution Approach 1:

The invention enables dynamic adjustment of the spectrometer's operational parameters. The entire assembly can be translated along the crystal axis to change the central Bragg angle, allowing access to different energy ranges. Additionally, the system can accommodate different crystals with various crystallographic spacings and angular specifications, providing adaptability across an expanded energy range from 0.547 to 16.8 keV while maintaining the focusing capability provided by the cylindrical geometry.

Inventive Principle:
Principle #15Dynamics

4Measurement precision

If conventional systems diffract from a single point on the crystal, then geometric focusing is achieved, but efficiency varies due to inconsistencies along the diffractor

Engineering Contradiction:
Improvegeometric focusingVSAvoiddiffraction efficiency
Core Design Contradiction:
Measurement precisionVSProductivity

Solution Approach 1:

The invention utilizes the entire active length of the cylindrically bent crystal for diffraction, rather than relying on a single point. The continuous curved surface of the crystal provides consistent diffraction efficiency along its length, as each segment of the crystal contributes to the focused signal at the detector. This continuous utilization of the crystal surface eliminates efficiency variations that would arise from using discrete points, maintaining both geometric focusing and consistent productivity across the diffracting surface.

Inventive Principle:
Principle #20Continuity of useful action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution provides a compact, cost-effective medium resolution spectrometer with improved energy resolution (10-100 eV) that simplifies operation by controlling a single motion, eliminating efficiency variations and enabling easy attachment to various detectors, while maintaining high throughput and versatility across different energy ranges.

Implementation Method 1

The x-ray spectrometer operates by using a diffractive crystal which, for any given angle, diffracts x-rays of a specific energy according to the Bragg equation (a): wavelength=2d sin Θ

Methodology Applied
Scientific EffectBragg diffraction: Bragg Diffraction

Implementation Method 2

The crystal is bent cylindrically around a horizontal axis, parallel to a direction of dispersion. The crystal provides focusing in a vertical direction.

Methodology Applied
Scientific EffectCylindrical focusing: Focusing

Data Source

PatentUS10672529B1Compact spectrometer focusing apparatus
Publication Date: 2020.06.02 THE RES FOUNDATION FOR THE STATE UNIV OF NEW YORK
  • US10672529B1 patent drawing
  • US10672529B1 patent drawing
  • US10672529B1 patent drawing

AI summary

A spectrometer focusing apparatus is provided that includes a hollow cylinder for x-rays to traverse a length thereof, a defracting element configured as a ring on an interior circumference of a portion of the hollow cylinder, at least one disk having an edge defining a circle aligned with the defracting element, and an aperture formed between the defracting element and the edge of the at least one disk.