Benzene-bis(dithioic) Acid Derivatives for Battery Electrodes

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Solution Overview

Problem

Current active electrode materials for lithium-ion batteries face challenges such as high costs, reduced energy density, and instability issues, particularly in hybrid and electric vehicles and photovoltaic applications, due to the need for large quantities of conventional conductors and inadequate redox potential.

Innovation Solution

The use of compounds with a specific formula, such as (1,4-benzene)-bis-lithium bisdithioate, which offer improved chemical, thermal, and electrochemical stability, high redox potential, and enhanced electronic and ionic transport properties, potentially reducing the reliance on conventional conductors and binders.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If conventional conductive materials like carbon black are used in large quantities to enable electron extraction from active material, then electrical conductivity is improved, but mass and volume energy density deteriorate

Engineering Contradiction:
Improveelectrical conductivityVSAvoidmass energy density
Core Design Contradiction:
ReliabilityVSQuantity of substance

Solution Approach 1:

The patent introduces a conductive polymer as an intermediary material that bridges the active material and conventional conductors. This polymer layer facilitates electron extraction from the active material while requiring significantly less conductor content than conventional approaches, thereby improving energy density without sacrificing electrical conductivity

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The patent changes the physical and chemical parameters of the electrode by incorporating conductive polymers with specific molecular structures and properties. This parameter change enables the system to achieve adequate electrical conductivity with reduced conductor content, resolving the contradiction between conductivity and energy density

Inventive Principle:
Principle #35Parameter changes

2Reliability

If large quantities of conventional conductors are added to active material, then electrical percolation is improved, but production cost increases

Engineering Contradiction:
Improveelectrical percolationVSAvoidproduction cost
Core Design Contradiction:
ReliabilityVSEase of manufacture

Solution Approach 1:

The conductive polymer serves as a cost-effective intermediary that provides the necessary electrical percolation pathway. By using this polymer mediator, the patent reduces the quantity of expensive conventional conductors needed, thereby lowering production costs while maintaining adequate electrical percolation

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The patent employs conductive polymers that can be synthesized at lower cost compared to conventional conductive materials. These polymers provide the necessary electrical pathways without requiring the expensive materials traditionally used, making the overall electrode manufacturing more cost-effective

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

3Strength

If additional binders are used to ensure adhesion of polymer material to current collector, then mechanical strength is improved, but mass energy density deteriorates

Engineering Contradiction:
Improvemechanical strengthVSAvoidmass energy density
Core Design Contradiction:
StrengthVSQuantity of substance

Solution Approach 1:

The patent merges the functions of the conductive polymer and the binder by designing a system where the conductive polymer itself provides adequate adhesion to the current collector. This merging eliminates or reduces the need for separate binder materials, thereby improving mass energy density while maintaining mechanical strength

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The conductive polymer is designed to perform multiple functions simultaneously: providing electrical conductivity, ensuring adhesion to the current collector, and contributing to mechanical strength. This multi-functionality reduces the need for additional specialized materials, improving energy density

Inventive Principle:
Principle #6Universality (Multi-functionality)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

These compounds enable the creation of electrodes with improved flexibility, stability, and performance, potentially lowering production costs and increasing energy density while maintaining mechanical strength and adhesion to current collectors.

Implementation Method 1

These lithium electrochemical generators conventionally operate on the principle of insertion or deinsertion (or intercalation-deintercalation) of lithium on at least one electrode

Methodology Applied
Scientific EffectIntercalation-deintercalation:

Implementation Method 2

the compounds according to the invention... have improved electronic and ionic transport properties... and also have a high redox potential

Methodology Applied
Scientific EffectRedox reactions: Redox Reactions

Implementation Method 3

the compounds according to the invention... offer improved chemical, thermal, and electrochemical stability, high redox potential, and enhanced electronic and ionic transport properties

Methodology Applied
Scientific EffectElectrical conduction: Conduction (electrical)

Implementation Method 4

the compounds according to the invention... offer improved chemical, thermal, and electrochemical stability, high redox potential, and enhanced electronic and ionic transport properties

Methodology Applied
Scientific EffectIonic conduction: Conduction (electrical)

Data Source

PatentEP3063127B1Material for an electrode of an organic battery comprising benzene-bis(dithioic) acid derivatives
Publication Date: 2017.12.13 COMMISSARIAT A LENERGIE ATOMIQUE ET AUX ENERGIES ALTERNATIVES
  • EP3063127B1 patent drawingFigure 1A~1B
  • EP3063127B1 patent drawingFigure 2A~2B
  • EP3063127B1 patent drawingFigure 3~4

AI summary

The present invention concerns the use, as an active electrode material, of compounds comprising at least one entity of formula (I): in which the phenyl group is substituted with one to four identical or different substituent(s) R, chosen from a hydrogen atom, a halogen atom chosen from fluorine, chlorine, bromine or iodine, a -C(=S)-S-C+ group, an -O-C+ group, an -S-C+ group, C+ being an alkali cation chosen from Li+, Na+ and K+, a (C1-C12) alkyl radical, a (C2-C12) alkenyl radical, a (C6-C14) aryl or heteroaryl radical; or two vicinal substituents R that can, if appropriate, be linked to each other to together form a 3- to 7-membered ring optionally including another heteroatom chosen from N, O or S; in the base or salt form; and the tautomeric forms of same. It also concerns an electrode material, an electrode and a lithium, sodium or potassium secondary battery, obtained from these compounds.