Beta-Sialon Fluorescent Material Surface Area Optimization

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Solution Overview

Problem

Current methods for producing β-sialon fluorescent materials do not adequately enhance light emission luminance, limiting their efficiency in applications such as lighting systems and liquid crystal display devices.

Innovation Solution

A method involving the preparation of a calcined β-sialon product, followed by grinding to achieve a specific surface area of 0.2 m2/g or more, and subsequent heat-treating, with the option to repeat grinding and heat-treating steps to ensure an average particle diameter of 40 μm or less, thereby optimizing the incorporation of activating elements and enhancing light emission intensity.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Illumination intensity

If conventional calcination methods are used to produce β-sialon fluorescent materials, then the production process is simple, but the light emission luminance is insufficient

Engineering Contradiction:
Improvelight emission luminanceVSAvoidproduction process complexity
Core Design Contradiction:
Illumination intensityVSDevice complexity

Solution Approach 1:

The patent applies preliminary action by performing grinding treatment to increase specific surface area before the final heat treatment step. This preliminary preparation of the calcined product ensures that subsequent heat treatment can achieve high light emission luminance more effectively, as the increased surface area improves reacting ability and activating element incorporation

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent applies parameter changes by controlling specific surface area (0.2 m²/g or more) and particle diameter (40 μm or less) as key parameters. By adjusting these physical parameters through grinding and heat treatment, the light emission luminance is significantly enhanced while maintaining a manageable production process

Inventive Principle:
Principle #35Parameter changes

2Illumination intensity

If the calcined product is not ground sufficiently, then the production process is fast, but the specific surface area is too low to enhance light emission intensity

Engineering Contradiction:
Improvelight emission intensityVSAvoidgrinding time
Core Design Contradiction:
Illumination intensityVSLoss of time

Solution Approach 1:

The patent applies parameter changes by setting specific thresholds for specific surface area (0.2 m²/g or more) and particle diameter (40 μm or less). These quantified parameters provide clear targets for the grinding process, enabling optimization of both grinding time and light emission intensity through controlled parameter adjustment

Inventive Principle:
Principle #35Parameter changes

3Manufacturing precision

If the particle diameter is not controlled, then the manufacturing process is simple, but the uniformity of fluorescent material performance is poor

Engineering Contradiction:
Improveparticle size uniformityVSAvoidprocess control complexity
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The patent applies parameter changes by establishing a maximum particle diameter threshold (40 μm or less) through controlled heat treatment. This parameter control ensures uniform particle size distribution and consistent fluorescent performance while maintaining relatively simple process control through well-defined thermal processing conditions

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method results in β-sialon fluorescent materials with significantly improved light emission intensity, as demonstrated by increased relative light emission intensity and uniform particle size distribution, enhancing their performance in lighting and display applications.

Implementation Method 1

heat-treating the ground product to obtain a heat-treated product

Methodology Applied
Scientific EffectHeat treatment: Heat Treatment

Implementation Method 2

β-sialon fluorescent material which is excited in a wide wavelength region of from near-ultraviolet light to blue light and has a peak light emission wavelength in the range of 520 nm or longer and 560 nm or shorter

Methodology Applied
Scientific EffectFluorescence: Fluorescence

Data Source

PatentUS11512250B2Method of producing β-sialon fluorescent material
Publication Date: 2022.11.29 NICHIA CORP
  • US11512250B2 patent drawing
  • US11512250B2 patent drawing
  • US11512250B2 patent drawing

AI summary

Provided is a method of producing a β-sialon fluorescent material having a high light emission intensity and an excellent light emission luminance. The method includes preparing a calcined product having a composition of β-sialon containing an activating element; grinding the calcined product to obtain a ground product; and heat-treating the ground product to obtain a heat-treated product. A specific surface area of the ground product is 0.2 m2/g or more.