Biaxially Textured Buffer Layers for HTS Film Production

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Solution Overview

Problem

The existing ion-beam assisted deposition (IBAD) processes for producing biaxially textured buffer layers for high-temperature superconducting (HTS) films are slow, expensive, and difficult to scale due to the need for thick films and sensitive nucleation control, limiting the production of superconducting tapes with high critical current densities.

Innovation Solution

A method involving separate buffer layers, where a first uniaxially textured buffer layer with out-of-plane texture is used, followed by an ion-beam induced in-plane texture in a second buffer layer, allowing for the deposition of a biaxially textured surface without the need for full ion-assist processing, enabling efficient and cost-effective production of HTS films with high critical current densities.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If ion-assist process is used to produce biaxial texture in buffer layer, then high critical current density is achieved, but production speed decreases and cost increases

Engineering Contradiction:
Improvecritical current densityVSAvoidproduction speed
Core Design Contradiction:
ReliabilityVSProductivity

Solution Approach 1:

The buffer layer is divided into two separate layers: a first buffer layer that provides out-of-plane texture without ion assistance, and a second buffer layer that receives ion-beam induced in-plane texture. This segmentation allows the ion-assist process to be applied only to the second layer, reducing overall processing time and cost while maintaining the high critical current density required for HTS films.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The first buffer layer is deposited in advance to establish the out-of-plane crystallographic texture before the ion-assist process is applied to the second buffer layer. This preliminary action prepares the substrate in a state that facilitates subsequent in-plane texturing, enabling faster and more cost-effective production while ensuring the final biaxial texture quality.

Inventive Principle:
Principle #10Preliminary action

2Manufacturing precision

If thick buffer layer is deposited with ion-assist process, then optimal biaxial texture is achieved, but deposition time increases and cost increases

Engineering Contradiction:
Improvebiaxial texture qualityVSAvoiddeposition time
Core Design Contradiction:
Manufacturing precisionVSLoss of time

Solution Approach 1:

The buffer layer thickness is segmented between two layers, allowing the ion-assist process to be concentrated on the second layer only. This reduces the total thickness requiring ion assistance, thereby decreasing deposition time and cost while achieving the necessary biaxial texture quality for HTS film growth.

Inventive Principle:
Principle #1Segmentation

3Manufacturing precision

If sub-10 nm nucleation control is employed for MgO IBAD deposition, then crystallographic texture is controlled, but process complexity increases and scalability decreases

Engineering Contradiction:
Improvecrystallographic texture controlVSAvoidprocess complexity
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The nucleation and texturing processes are segmented between two buffer layers. The first buffer layer establishes out-of-plane orientation without requiring precise nucleation control, while the second buffer layer receives ion-beam induced texturing. This segmentation eliminates the need for complex in-situ monitoring techniques, simplifying the process and enabling large-scale production.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The complex in-situ monitoring and precise nucleation control mechanism is replaced with a simpler ion-beam induced texturing process applied to the second buffer layer. This substitution eliminates the need for reflection high energy electron diffraction monitoring and other complex control systems, making the process suitable for large-scale production.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enables the production of biaxially textured articles with high critical current densities, such as superconductor tapes, efficiently and economically, eliminating the need for extensive ion-assist processing and improving the scalability of HTS film production.

Implementation Method 1

The second buffer film is then bombarded with an ion beam. The ion beam induces in-plane texture in a surface of the second buffer film to form a biaxially textured surface.

Methodology Applied
Scientific EffectIon-beam assisted deposition: Ion Beam

Data Source

PatentUS7569521B2Method of producing biaxially textured substrates and related articles, devices and systems
Publication Date: 2009.08.04 UNIV OF FLORIDA RESEARCH FOUNDATION INC
  • US7569521B2 patent drawing
  • US7569521B2 patent drawing
  • US7569521B2 patent drawing

AI summary

A biaxially textured article includes a substrate, a first buffer layer disposed on the substrate, the first buffer layer having uniaxial crystal texture characterized by out-of-plane texture with no significant in-plane crystallographic texture. A metal comprising second buffer layer is disposed on the first buffer layer, the second buffer layer having a biaxially textured surface. An electronically active layer, such as a superconductor layer, can be disposed on the second buffer film. Ion-beam assisted processes can be used to biaxially texture the surface of the second buffer film after its deposition.