Bio-based Two-Part Polyurethane Adhesive Formulation

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Solution Overview

Problem

Current urethane adhesives are predominantly petroleum-based, making them susceptible to price fluctuations and availability issues, and they often contain high levels of Volatile Organic Compounds (VOCs), whereas there is a need for bio-based adhesives with minimal VOCs and the ability to be formulated for specific physical properties.

Innovation Solution

A two-part urethane adhesive composition where the B side is partially derived from plant oils, such as soybean oil, with a high proportion of hydroxylated soybean oil and optional phosphated soybean oil, along with catalysts and surfactants, to minimize reactive organic isocyanate usage and maximize bio-based components, while maintaining low VOC levels.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If petroleum-based components are used in urethane adhesives, then the adhesive can be produced with established processes and consistent performance, but the adhesive becomes subject to price fluctuation and availability issues

Engineering Contradiction:
Improveadhesive performance consistencyVSAvoidpetroleum availability
Core Design Contradiction:
ReliabilityVSQuantity of substance

Solution Approach 1:

The patent changes the chemical composition parameters by replacing petroleum-based polyols with bio-based alternatives derived from vegetable oils, while adjusting the molecular structure and hydroxyl content to maintain adhesive performance consistency

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates a composite adhesive system combining bio-based polyols from vegetable oils with isocyanate components, forming a new material composition that maintains urethane adhesive properties while reducing petroleum dependence

Inventive Principle:
Principle #40Composite materials

2Strength

If traditional urethane adhesive formulations are used, then the adhesive provides adequate bonding performance, but the Volatile Organic Content exceeds 2 percent

Engineering Contradiction:
Improveadhesive bonding strengthVSAvoidVolatile Organic Content
Core Design Contradiction:
StrengthVSObject-generated harmful factors

Solution Approach 1:

The patent changes the formulation parameters by selecting polyols with specific molecular weights and hydroxyl numbers from bio-based sources, which inherently reduce VOC content while maintaining curing reaction efficiency and bond strength

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent converts the potential disadvantage of using less common bio-based materials into a benefit by achieving both low VOC content and high bond strength, transforming an alternative formulation approach into a superior performance adhesive

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

3Quantity of substance

If bio-based components are used to replace petroleum-based polyols, then the adhesive reduces dependence on petroleum sources, but the adhesive may have inconsistent physical properties

Engineering Contradiction:
Improvebio-based contentVSAvoidadhesive physical properties
Core Design Contradiction:
Quantity of substanceVSStability of the object's composition

Solution Approach 1:

The patent establishes specific parameter ranges for bio-based polyols including hydroxyl number, molecular weight, and fatty acid composition to ensure consistent physical properties across different batches and applications

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent uses carefully selected bio-based polyols as intermediaries that bridge the gap between renewable vegetable oil sources and the required performance specifications of urethane adhesives, ensuring compositional stability

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The adhesive composition achieves strong adhesion and flexibility, with minimal VOCs, and can be formulated for various applications, including roofing, construction, and insulation, with rapid cure times and high bio-based content, reducing dependence on petroleum sources and environmental impact.

Implementation Method 1

These are usually methylene diphenyl diisocyanate for the A side, and a polyether such as polypropylene glycol or a polyester polyol such as ethylene adipate diol for the B side

Methodology Applied
Scientific EffectPolyaddition reaction: Chemical Bonding

Implementation Method 2

along with catalysts and surfactants, to minimize reactive organic isocyanate usage

Methodology Applied
Scientific EffectCatalysis: Catalysis

Implementation Method 3

along with catalysts and surfactants

Methodology Applied
Scientific EffectSurface tension reduction: Surfactant

Data Source

PatentUS20240043727A1Bio-based, multipurpose two-part adhesive
Publication Date: 2024.02.08 VIRIDIS TECH LLC

AI summary

A polyurethane adhesive including an A side component having a reactive organic diisocyanate and a B side component having hydroxylated plant-based oil, phosphated plant-based oil, and optionally, at least one of a catalyst, a surfactant, water, and a trace amount of A side component.