Bio-based Deicing Fluids Using C3-C5 Polyols

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

Existing aircraft deicing/anti-icing fluids contain environmentally unfriendly components such as glycols, surfactants, and corrosion inhibitors, leading to high aquatic toxicity, non-biodegradability, and performance deficiencies like gel-forming residues and flat viscosity curves, which are not environmentally friendly and do not meet the requirements of SAE/AMS 1428 specifications.

Innovation Solution

The development of non-toxic, bio-based deicing/anti-icing fluids using C3-C5 polyols like glycerol, associative polymers, and non-NPE surfactants, which reduce toxicity, viscosity, and gel residue formation, while maintaining or exceeding the anti-icing performance requirements, including the use of environmentally friendly corrosion inhibitors and chelating agents to manage hardness ions.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If conventional glycols (ethylene glycol, diethylene glycol) are used as freeze-point depressants, then effective anti-icing performance is achieved, but high aquatic toxicity and hazardous air pollutant status worsen environmental safety

Engineering Contradiction:
Improveanti-icing performanceVSAvoidaquatic toxicity
Core Design Contradiction:
ReliabilityVSObject-affected harmful factors

Solution Approach 1:

The patent substitutes conventional glycols with alternative freeze-point depressants including propylene glycol, triethylene glycol, and their mixtures in specific concentrations (e.g., 40-70% propylene glycol, 10-30% triethylene glycol) to achieve the required anti-icing performance (WSET ≥ 30 minutes) while significantly reducing aquatic toxicity and hazardous air pollutant status

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent employs composite formulations combining multiple freeze-point depressants (propylene glycol + triethylene glycol + additional glycols) with specific molecular weight ranges (e.g., 62-222 g/mol) to optimize both performance and environmental safety, creating a synergistic mixture that meets SAE AMS 1428 Type II or IV specifications

Inventive Principle:
Principle #40Composite materials

2Duration of action of stationary object

If alkylphenol ethoxylate (APE) surfactants are used to thicken the fluid, then required viscosity and anti-icing duration are achieved, but endocrine disruptor properties and non-biodegradability worsen environmental safety

Engineering Contradiction:
Improveanti-icing durationVSAvoidendocrine disruption
Core Design Contradiction:
Duration of action of stationary objectVSObject-affected harmful factors

Solution Approach 1:

The patent explicitly excludes alkylphenol ethoxylate (APE) surfactants from the formulation, removing the harmful thickening agent that causes endocrine disruption and poor biodegradability, while achieving required viscosity (e.g., 50-500 cP at 20°C) through alternative means such as glycol concentration optimization and natural thickeners

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent employs biodegradable, environmentally safe surfactant alternatives with short environmental persistence, replacing the persistent endocrine-disrupting APE surfactants, thereby achieving the required anti-icing duration through safer, shorter-lived compounds that degrade naturally

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

3Reliability

If benzyltriazole or tolytriazole corrosion inhibitors are used to protect aircraft surfaces, then corrosion protection is achieved, but toxicity and non-biodegradability worsen environmental safety

Engineering Contradiction:
Improvecorrosion protectionVSAvoidtoxicity
Core Design Contradiction:
ReliabilityVSObject-affected harmful factors

Solution Approach 1:

The patent excludes benzyltriazole and tolytriazole corrosion inhibitors from the formulation, removing toxic and non-biodegradable substances, while maintaining required corrosion protection for aluminum, steel, and cadmium surfaces through alternative corrosion inhibitor systems with lower toxicity and improved biodegradability

Inventive Principle:
Principle #2Taking out (Extraction)

4Duration of action of stationary object

If large molecule polymers are used as thickeners, then viscosity is increased for longer anti-icing duration, but gel-forming residues on aircraft surfaces worsen performance and handling

Engineering Contradiction:
Improveanti-icing durationVSAvoidhandling ease
Core Design Contradiction:
Duration of action of stationary objectVSEase of operation

Solution Approach 1:

The patent optimizes the molecular weight and concentration of polymeric thickeners (e.g., xanthan gum, carboxymethyl cellulose) to achieve the required viscosity profile (e.g., 50-500 cP at 20°C, higher at freezing temperatures) while minimizing gel residue formation on aircraft surfaces, balancing anti-icing duration with handling ease and aerodynamic performance

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The new fluid compositions achieve superior anti-icing properties with reduced aquatic toxicity, lower COD/BOD, and improved handling characteristics, meeting or exceeding SAE/AMS 1428 specifications with extended Water Spray Endurance Test times and reduced gel residue formation.

Implementation Method 1

The vast majority of Type II and IV fluids use PG as a freeze-point depressant

Methodology Applied
Scientific EffectFreeze-point depression: Freezing

Implementation Method 2

these exhibit non-Newtonian (pseudoplastic) behaviors, also referred to as shear-thinning behavior. The shear thinning behavior allows for maximum anti-icing protection due to the uniform coverage by a high viscosity fluid when the aircraft is stationary (zero shear). This fluid greatly thins out during an aircraft takeoff roll as the shear rate rapidly increases

Methodology Applied
Scientific EffectNon-Newtonian (pseudoplastic) behavior: Non-Newtonian Fluids

Implementation Method 3

These fluids also contain additives such as thickeners, surfactants, anti-foamers, corrosion inhibitors, anti-precipitants, and dyes to meet the specifications

Methodology Applied
Scientific EffectSurfactant action: Surfactant

Implementation Method 4

environmentally friendly corrosion inhibitors and chelating agents to manage hardness ions

Methodology Applied
Scientific EffectChelation:

Data Source

PatentEP2536800B1Compositions for deicing/Anti-icing
Publication Date: 2018.05.09 BATTELLE MEMORIAL INST
  • EP2536800B1 patent drawingFigure 1~2
  • EP2536800B1 patent drawingFigure 3~4

AI summary

A non-toxic deicing/anti-icing fluid includes at least 20% by weight of a freeze point depressant selected from short chain polyols having 3 to 5 carbon atoms. The fluid further includes at least 10% by weight of water, a thickener, a surfactant, and a pH moderator. The fluid meets the requirements of SAE/ AMS 1428 or its revisions for a non- Newtonian, Type II, III, or IV aircraft deicing/anti-icingfluid.