Bio-Based LOHC Mixtures for Low-Energy Hydrogen Release

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Solution Overview

Problem

Existing hydrogen carriers, such as aromatic hydrocarbons and heteroaromatic compounds, are expensive due to the use of scarce noble metals, inefficient in energy consumption, and derived from non-renewable resources, limiting their decarbonization potential.

Innovation Solution

Development of hydrogenated organic liquids (LOHCs) synthesized from renewable bio-based resources, using less energy-intensive dehydrogenation processes and alternative catalysts like copper and nickel, allowing reversible hydrogenation and dehydrogenation without noble metals.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If conventional hydrogen carriers (aromatic hydrocarbons, heteroaromatic compounds) are used, then hydrogen storage and transport capability is achieved, but cost increases due to use of scarce noble metals

Engineering Contradiction:
Improvehydrogen storage capacityVSAvoidcost
Core Design Contradiction:
Quantity of substanceVSEase of manufacture

Solution Approach 1:

The patent replaces expensive noble metal catalysts (platinum, palladium, rhodium) with cheaper alternative catalysts based on abundant metals such as nickel, copper, iron, and cobalt. These alternative catalysts achieve comparable catalytic activity for hydrogenation and dehydrogenation reactions, significantly reducing the cost of hydrogen carrier systems while maintaining functional performance.

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

Solution Approach 2:

The patent modifies reaction parameters including temperature, pressure, and catalyst composition to optimize the performance of alternative non-noble metal catalysts. By adjusting these parameters, the system achieves efficient hydrogen storage and release cycles using cost-effective catalysts, resolving the contradiction between hydrogen capacity and manufacturing cost.

Inventive Principle:
Principle #35Parameter changes

2Quantity of substance

If conventional LOHC dehydrogenation processes are used, then hydrogen is released, but energy consumption increases

Engineering Contradiction:
Improvehydrogen releaseVSAvoidenergy consumption
Core Design Contradiction:
Quantity of substanceVSUse of energy by moving object

Solution Approach 1:

The patent optimizes dehydrogenation reaction parameters including temperature, pressure, and catalyst composition to reduce energy consumption. By using alternative catalysts and adjusting operational parameters, the system achieves efficient hydrogen release at lower energy input compared to conventional processes.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent implements continuous hydrogenation-dehydrogenation cycles where the hydrogen carrier is repeatedly used. The dehydrogenated carrier is continuously regenerated through hydrogenation, creating a sustainable loop that reduces overall energy consumption per unit of hydrogen released while maintaining continuous operational capability.

Inventive Principle:
Principle #20Continuity of useful action

3Quantity of substance

If conventional LOHCs derived from non-renewable resources are used, then hydrogen transport is achieved, but decarbonization potential is limited

Engineering Contradiction:
Improvehydrogen transport capacityVSAvoidcarbon emissions
Core Design Contradiction:
Quantity of substanceVSObject-generated harmful factors

Solution Approach 1:

The patent modifies the feedstock source from conventional fossil-based aromatic hydrocarbons to renewable biomass-derived platform chemicals such as furfural, 5-hydroxymethylfurfural (HMF), and levulinic acid. This parameter change in原料 sourcing enables the production of renewable LOHCs that can be sustainably hydrogenated and dehydrogenated, achieving hydrogen transport while reducing dependence on non-renewable resources and lowering carbon emissions.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The new LOHCs achieve high hydrogen concentration and efficiency with reduced energy consumption, utilizing bio-based resources and less expensive catalysts, enhancing decarbonization and cost-effectiveness.

Implementation Method 1

The hydrogen-rich organic liquid is then dehydrogenated in a second reaction to regenerate the hydrogen and the hydrogen-deficient organic liquid. Advantageously, these LOHCs are thus capable of being reversibly hydrogenated and dehydrogenated in the presence of a catalyst.

Methodology Applied
Scientific EffectHydrogenation: Hydrogenation

Implementation Method 2

The hydrogen-rich organic liquid is then dehydrogenated in a second reaction to regenerate the hydrogen and the hydrogen-deficient organic liquid.

Methodology Applied
Scientific EffectDehydrogenation: Chemical Bonding

Implementation Method 3

Advantageously, these LOHCs are thus capable of being reversibly hydrogenated and dehydrogenated in the presence of a catalyst.

Methodology Applied
Scientific EffectCatalysis: Catalysis

Data Source

PatentEP4419477B1Mixtures of liquid organic hydrogen carriers, uses thereof for transporting and storing hydrogen, and hydrogen generation methods using same
Publication Date: 2025.12.17 COMMISSARIAT A LENERGIE ATOMIQUE ET AUX ENERGIES ALTERNATIVES
  • EP4419477B1 patent drawingFigure 1~2
  • EP4419477B1 patent drawingFigure 3~4
  • EP4419477B1 patent drawing

AI summary

The invention relates to mixtures of liquid organic hydrogen carriers (LOHC) and to pairs consisting of an LOHC mixture and corresponding dehydrogenated LOHC(s). The invention also relates to the uses of said mixtures for transporting and storing hydrogen as well as to hydrogen generation methods using same.