Biofuel Production via High-Pressure Homogenization

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Solution Overview

Problem

Conventional methods for producing biodiesel, such as transesterification and hydrotreating, face challenges including slow reaction times, generation of unwanted byproducts, and less desirable cold flow properties, which hinder efficient and safe biofuel production.

Innovation Solution

A method and system for manufacturing biofuel involving a high-pressure homogenization process using a renewable energy feedstock, alcohol, and catalyst, where the mixture is processed at pressures greater than 400 kilogram-force per square centimeter to create a stable biofuel product.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If transesterification is used to produce biodiesel, then the chemical reaction can proceed with available catalysts and reactants, but the reaction time becomes excessively long (0.5 to 8 hours) and unwanted byproducts (glycerol, water, soaps, caustic agents) are generated

Engineering Contradiction:
Improvereaction timeVSAvoidbyproduct formation
Core Design Contradiction:
ProductivityVSObject-generated harmful factors

Solution Approach 1:

The patent applies parameter changes by using high pressure (greater than 400 kg/cm²) to alter the physical state and reaction kinetics of the transesterification process. This pressure parameter change accelerates the reaction rate significantly, reducing reaction time from hours to minutes, while also improving the separation and removal of byproducts like glycerol and water, thus resolving both the productivity and harmful factors contradictions.

Inventive Principle:
Principle #35Parameter changes

2Reliability

If hydrotreating is used to remove sulfur impurities, then the fuel can meet ASTM diesel standards, but the cold flow properties become less desirable

Engineering Contradiction:
Improvefuel standard complianceVSAvoidcold flow properties
Core Design Contradiction:
ReliabilityVSEase of operation

Solution Approach 1:

The patent uses parameter changes by applying high pressure to the transesterification process to produce a biofuel that inherently maintains better cold flow properties compared to conventional hydrotreating. The pressure-induced reaction pathway creates a different molecular structure in the biodiesel that preserves cold flow characteristics while still achieving sulfur removal and ASTM standard compliance, thus resolving the contradiction between reliability and ease of operation.

Inventive Principle:
Principle #35Parameter changes

3Speed

If excess reactants and catalysts are used to drive the transesterification reaction faster, then the reaction rate increases, but more harmful byproducts (alcohols, soaps, caustic agents) are generated

Engineering Contradiction:
Improvereaction rateVSAvoidbyproduct concentration
Core Design Contradiction:
SpeedVSObject-generated harmful factors

Solution Approach 1:

The patent resolves this contradiction by changing the pressure parameter to greater than 400 kg/cm², which accelerates the reaction rate through pressure-induced kinetic enhancement rather than through excess reactants. This pressure-driven rate increase achieves fast reaction speeds without requiring excessive catalysts or reactants, thereby minimizing the formation of harmful byproducts like soaps and caustic agents.

Inventive Principle:
Principle #35Parameter changes

4Ease of manufacture

If conventional transesterification is used, then the process can be implemented with standard equipment, but the production efficiency remains low due to slow reaction rates and extensive byproduct removal requirements

Engineering Contradiction:
Improveprocess implementabilityVSAvoidproduction efficiency
Core Design Contradiction:
Ease of manufactureVSProductivity

Solution Approach 1:

The patent maintains ease of manufacture by using standard transesterification chemistry and equipment, but dramatically improves productivity through the parameter change of applying high pressure (greater than 400 kg/cm²). This pressure enhancement accelerates the reaction from hours to minutes and improves byproduct separation efficiency, achieving high production efficiency without requiring completely new or complex manufacturing systems.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enhances production efficiency, reduces byproduct formation, and improves biofuel characteristics, allowing for faster production of a stable biofuel that can be used in combustion engines without harming the engine, while also being adaptable to various feedstocks and processing conditions.

Implementation Method 1

homogenizing the blend at a pressure greater than 400 kilogram-force per square centimeter (Kg/cm2)

Methodology Applied
Scientific EffectHigh-pressure homogenization: Compression

Data Source

PatentUS9080117B2Biofuel production method and system
Publication Date: 2015.07.14 GER ENTERPRISES
  • US9080117B2 patent drawing
  • US9080117B2 patent drawing
  • US9080117B2 patent drawing

AI summary

In an embodiment of the present invention, a renewable energy fuel is prepared by a process including the steps of: a) providing a renewable energy feedstock; b) providing an alcohol; c) providing a catalyst; d) mixing (a), (b), and (c) to form a blend; and e) homogenizing the blend at a pressure greater than 400 kilogram-force per square centimeter (Kg/cm2).