Biogas Purification Culture Medium for H2S Removal

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Solution Overview

Problem

Current biological methods for biogas purification lack effectiveness on an industrial scale and result in elemental sulphur deposition, which requires regular removal, and existing solutions fail to efficiently remove hydrogen sulphide and carbon dioxide from biogas, leading to suboptimal biogas composition and environmental concerns.

Innovation Solution

A microbiological culture medium composed of KH2PO4, MgCl2, Ca(NO3)2, FeSO4, ZnSO4, MnCl2, CoCl2, CuSO4, and (NH4)2MoO4 is used to cultivate a consortium of microorganisms that form a specific biofilm in a biofilter, effectively converting hydrogen sulphide into elemental sulphur or sulphates, with a pH range of 5 to 8 and a sprinkling volume of 5-500 L/h, ensuring efficient biogas purification without carbon source addition.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of manufacture

If conventional biological methods are used for biogas purification, then capital outlays are reduced, but purification effectiveness is insufficient and elemental sulphur deposition occurs

Engineering Contradiction:
Improvecapital outlaysVSAvoidpurification effectiveness
Core Design Contradiction:
Ease of manufactureVSReliability

Solution Approach 1:

The patent changes the chemical composition parameters of the culture medium by replacing traditional carbon sources (NaHCO3, sodium acetate) with a nitrogen-based nutrient composition (NH4Cl, (NH4)2SO4, KNO3) and adjusting concentrations of phosphates, sulfates, and trace elements. This parameter change enables microorganisms to assimilate carbon from CO2 while maintaining high H2S removal efficiency and preventing elemental sulphur deposition

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent converts the harmful accumulation of elemental sulphur into a beneficial process by modifying the culture medium to promote complete oxidation of H2S to sulphates rather than partial oxidation to elemental sulphur. The adjusted nutrient composition directs microbial metabolism toward sulphate production, eliminating the need for sulphur removal operations

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

2Duration of action of stationary object

If carbon sources are added to the culture medium, then microorganism growth is supported, but CO2 removal capability is lost

Engineering Contradiction:
Improvemicroorganism growthVSAvoidCO2 removal capability
Core Design Contradiction:
Duration of action of stationary objectVSProductivity

Solution Approach 1:

The patent extracts and removes traditional carbon sources (NaHCO3, sodium acetate, yeast extract) from the culture medium composition. By eliminating these exogenous carbon sources, the system forces microorganisms to rely on CO2 assimilation for growth, thereby maintaining CO2 removal capability while supporting sustained microbial activity through nitrogen-based nutrients

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent makes the culture medium universally supportive of microorganisms that can fix CO2 by providing a balanced nutrient composition with nitrogen, phosphorus, sulfur, and trace elements that meets the diverse nutritional requirements of CO2-assimilating bacteria. This multi-functional medium supports both growth and CO2 removal functions simultaneously

Inventive Principle:
Principle #6Universality (Multi-functionality)

3Productivity

If heterotrophic microorganisms are used, then H2S removal is achieved, but CO2 binding capability is lost

Engineering Contradiction:
ImproveH2S removal efficiencyVSAvoidCO2 binding capability
Core Design Contradiction:
ProductivityVSAdaptability or versatility

Solution Approach 1:

The patent changes the selective parameter of the culture medium by adjusting the carbon-to-nitrogen ratio to zero (no exogenous carbon) and optimizing nitrogen sources (NH4Cl, (NH4)2SO4, KNO3) and phosphorus compounds. This parameter change creates selective pressure that favors autotrophic and facultative autotrophic microorganisms capable of CO2 fixation while maintaining H2S oxidation capability

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach achieves 97-100% hydrogen sulphide reduction efficiency, minimizing sulphur production and deposit volumes, maintaining stable pH, and producing biogas parameters comparable to natural gas, while reducing maintenance costs and environmental impact.

Implementation Method 1

aerobic forms of nitrogen... in the presence of aerobic forms of nitrogen... H2S was removed from waste gases by an activated carbon bioreactor with the help of a pure culture of T. denitrificans

Methodology Applied
Scientific EffectAerobic oxidation: Oxidation

Implementation Method 2

as the culture medium contains in its composition a source of carbon the microorganisms will not assimilate it from CO2

Methodology Applied
Scientific EffectCarbon fixation: Photosynthesis

Implementation Method 3

KH2PO4 100 g/500 L, MgCl2 x6H2O 50 g/500 L, Ca(NO3)2 x4H2O 50 g/500 L and FeSO4 x7H2O 40 g/500 L and trace elements

Methodology Applied
Scientific EffectDissolution: Solvation

Data Source

PatentEP3000872B1Microbiological medium for a microbiological consortium applied in the technology of biological purification of biogas
Publication Date: 2019.09.18 POLITECHNA LODZKA
  • EP3000872B1 patent drawingFigure 1

AI summary

A microbiological culture medium for the consortium of microorganisms, used in the technology of biological biogas purification, containing in its composition KH2PO4 (from 0.1 to 50 g/L), MgCl×6H2O (from 0.01 to 50 g/L), Ca(NO3)×4H2O (from 0.1 to 1000 g/L) and FeSO4×7H2O (from 0.01 to 50 g/L) and tap water.