Biomass Delignification via Acid Peroxide Capping

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Solution Overview

Problem

Current biomass delignification processes are inefficient, energy-intensive, and difficult to scale, leading to marginal yields and excessive processing costs, as they often damage cellulose and lignin, making it challenging to produce high-quality cellulose and lignin products for industrial applications.

Innovation Solution

A composition comprising an acid, a peroxide, and a capping agent is used for delignification at low temperatures and atmospheric pressure, which prevents further depolymerization of lignin and preserves its integrity, allowing for the separation of lignin from cellulose without degrading the cellulose fibers.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If conventional delignification processes are used to remove lignin from biomass, then lignin removal efficiency is improved, but cellulose integrity is damaged and processing costs increase

Engineering Contradiction:
Improvelignin removal efficiencyVSAvoidcellulose integrity
Core Design Contradiction:
Quantity of substanceVSStability of the object's composition

Solution Approach 1:

A capping agent is introduced as an intermediary substance that selectively binds to lignin fragments during delignification. This mediator allows lignin to be removed while preventing unwanted side reactions that would damage cellulose, thus resolving the contradiction between lignin removal efficiency and cellulose integrity

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The patent employs peroxide-based oxidation systems with controlled parameters (temperature, concentration, time) to achieve selective lignin depolymerization. By carefully controlling these parameters, the process removes lignin effectively while maintaining cellulose structure, resolving the contradiction between removal efficiency and structural preservation

Inventive Principle:
Principle #35Parameter changes

2Quantity of substance

If conventional delignification processes are used to separate lignin from cellulose, then delignification effectiveness is improved, but energy consumption increases

Engineering Contradiction:
Improvedelignification effectivenessVSAvoidenergy consumption
Core Design Contradiction:
Quantity of substanceVSUse of energy by moving object

Solution Approach 1:

The patent replaces energy-intensive mechanical and thermal delignification methods with a chemical oxidation system using peroxides. This substitution achieves effective lignin removal through chemical reactions at lower temperatures, significantly reducing energy consumption while maintaining delignification effectiveness

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Solution Approach 2:

Peroxide-based strong oxidants are used to accelerate the depolymerization of lignin at relatively low temperatures. This approach achieves rapid and effective delignification without requiring the high energy inputs needed by conventional thermal or mechanical processes

Inventive Principle:
Principle #38Strong oxidants (Accelerated oxidation)

3Quantity of substance

If conventional delignification processes are used to remove lignin, then lignin separation is improved, but processing costs increase

Engineering Contradiction:
Improvelignin separationVSAvoidprocessing cost
Core Design Contradiction:
Quantity of substanceVSEase of manufacture

Solution Approach 1:

The capping agent that binds to lignin fragments can be recovered and reused in subsequent delignification cycles. This recovery and reuse strategy reduces the cost of processing by minimizing the consumption of chemical reagents, thereby reducing overall processing costs while maintaining effective lignin separation

Inventive Principle:
Principle #34Discarding and recovering

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This method achieves substantial lignin removal with minimal cellulose loss, maintaining the integrity of lignin and cellulose, reducing energy consumption, and environmental impact, making it a more viable and cost-effective alternative to traditional pulping processes.

Implementation Method 1

a peroxide... which prevents further depolymerization of lignin

Methodology Applied
Scientific EffectOxidation: Oxidation

Implementation Method 2

A composition comprising an acid, a peroxide, and a capping agent is used for delignification

Methodology Applied
Scientific EffectHydrolysis: Hydrolysis

Data Source

PatentUS12252844B2Approach to biomass delignification
Publication Date: 2025.03.18 SIXRING INC

AI summary

Method of delignification of plant material, said method comprising: providing said plant material comprising cellulose fibres and lignin; exposing said plant material requiring to a composition comprising:an acid;a capping agent; anda peroxide;for a period of time sufficient to remove substantially all (at least 80%) of the lignin present on said plant material. Also disclosed are compositions to accomplish such delignification and processes using such.