Biomass Fractionation via Mild Refining and Chemical Treatment

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Solution Overview

Problem

Current pretreatment methods for lignocellulosic biomass, such as mechanical pulping, are energy-intensive and inefficient in separating hemicellulose and lignin, limiting the production of value-added bioproducts and biofuels.

Innovation Solution

A low-pressure mechanical refining process combined with mild chemical treatment to disintegrate lignocellulosic biomass, facilitating the separation and fractionation of hemicellulose, cellulose, and sulfur-free lignin, while minimizing energy consumption and chemical use.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If mechanical pulping is used for lignocellulosic biomass pretreatment, then fiber separation is achieved, but energy consumption increases significantly (up to 4000 kWh/t)

Engineering Contradiction:
Improvefiber separation efficiencyVSAvoidenergy consumption
Core Design Contradiction:
ProductivityVSUse of energy by moving object

Solution Approach 1:

The patent divides the biomass processing into distinct stages: low-energy mechanical refining for initial fiber separation, followed by chemical treatment for hemicellulose removal and lignin modification. This segmentation allows each stage to perform its specific function efficiently without requiring excessive energy at any single step.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The patent replaces high-energy mechanical pulping with a combination of low-energy mechanical refining followed by chemical treatment. The chemical processes (alkaline extraction, enzymatic treatment) substitute for the mechanical force that would otherwise be required to achieve complete fiber separation and component delignification.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

2Productivity

If conventional mechanical refining is used, then biomass is processed, but hemicellulose and lignin separation is inefficient

Engineering Contradiction:
Improvebiomass processing rateVSAvoidcomponent separation quality
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

The patent systematically extracts different biomass components through targeted chemical treatments: alkaline extraction removes hemicellulose, enzymatic treatment targets lignin, and organic solvent extraction isolates lignin and waxes. Each extraction step is designed to selectively remove specific components while preserving the cellulose structure.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent applies different chemical treatments to different aspects of the biomass processing: alkaline conditions for hemicellulose removal, enzymatic conditions for lignin modification, and organic solvents for lignin extraction. Each treatment is optimized for its specific target component, achieving high separation quality without compromising overall processing efficiency.

Inventive Principle:
Principle #3Local quality

3Productivity

If high chemical concentrations are used for pretreatment (e.g., 8-10% bisulfite, 1.8-3.7% sulfuric acid), then hydrolysis efficiency is enhanced, but chemical consumption and environmental impact increase

Engineering Contradiction:
Improvehydrolysis efficiencyVSAvoidchemical consumption
Core Design Contradiction:
ProductivityVSLoss of substance

Solution Approach 1:

The patent uses mild chemical concentrations (0.05-2% NaOH, 0.1-1% H2O2, 0.1-1% enzymes) and optimizes other parameters such as temperature (40-100°C), time (1-24 hours), and pH to achieve effective pretreatment. By changing the parameter组合 rather than relying on high chemical concentrations alone, the process achieves good hydrolysis efficiency with reduced chemical consumption.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent introduces intermediate treatment steps between mechanical refining and hydrolysis: alkaline treatment as an intermediary to remove hemicellulose and open up the cellulose structure, followed by enzymatic treatment as another intermediary to modify lignin. These intermediate steps facilitate subsequent hydrolysis without requiring high concentrations of harsh chemicals.

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This process enhances biofuel yields, produces high-quality sulfur-free lignin, and generates multiple value-added bioproducts with minimal refining energy and chemical input, making it a 'green' bioconversion method that can be easily integrated into existing mechanical pulp mills.

Implementation Method 1

mechanically refining the lignocellulosic biomass at a biomass consistency of 20% to 50% at 720 to 4320 MJ/t (200 to 1200 kWh/t) and a pressure of 100 to 600 kPa (1-6 bars)

Methodology Applied
Scientific EffectMechanical force: Mechanical Force

Implementation Method 2

subjecting the biomass to a chemical treatment using a mild chemical selected from the group of mild acids and alkalis, enzymes and oxidants at a temperature in the range of 20 to 145°C for 1 to 30 minutes

Methodology Applied
Scientific EffectChemical treatment:

Implementation Method 3

subjecting the biomass to a chemical treatment using a mild chemical selected from the group of mild acids and alkalis, enzymes and oxidants at a temperature in the range of 20 to 145°C for 1 to 30 minutes

Methodology Applied
Scientific EffectHeating: Heating

Data Source

PatentEP3388470B1Biomass fractionation process for bioproducts
Publication Date: 2024.04.17 FPINNOVATIONS INC
  • EP3388470B1 patent drawingFigure 1
  • EP3388470B1 patent drawingFigure 2
  • EP3388470B1 patent drawingFigure 3

AI summary

A fractionation process for producing value-added products from a lignocellulosic biomass, comprises: a) mechanically refining the lignocellulosic biomass under mild refining conditions to form a refined biomass pulp with enhanced susceptibility to separation of hemicellulose, cellulose and lignin, and enhanced digestibility of carbohydrates in hydrolysis b) separating hemicellulose and sulfur- free high-quality lignin from cellulose in the refined biomass, and, optionally c) producing various bioproducts from the above said process.