Biorenewable Processing Aid for Oxygen Barrier Sealing Elements

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Solution Overview

Problem

Thermoplastic elastomer sealing elements face challenges in achieving desirable oxygen barrier properties without contributing to the taste or odor of packaged products, while also being easily processable and resistant to high temperatures, as existing solutions like mineral oil and silicone oil either migrate or reduce barrier performance.

Innovation Solution

A sealing element composition comprising a styrenic block copolymer, a biorenewable processing aid with a crystalline melting range of 30-80°C, and an isobutylene-containing polymer or butyl rubber, which acts as both a processing aid and barrier synergist, enhancing oxygen barrier performance and processability.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of manufacture

If mineral oil plasticizer is added to improve processability, then ease of manufacture is improved, but harmful factors (odor, taste, migration) are generated

Engineering Contradiction:
ImproveprocessabilityVSAvoidodor and taste
Core Design Contradiction:
Ease of manufactureVSObject-generated harmful factors

Solution Approach 1:

The patent replaces conventional mineral oil plasticizers with biorenewable processing aids derived from natural sources (vegetable oils, animal fats). These biorenewable materials serve as temporary processing aids that can be easily removed or degraded, leaving no harmful residues in the final product. The processing aids improve manufacturability during extrusion and molding but do not contribute to odor or taste in the final sealing element.

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

Solution Approach 2:

The biorenewable processing aids act as intermediary substances that facilitate the processing of the sealing element composition without becoming permanent components of the final product. These intermediaries enable proper mixing and forming during manufacturing but are designed to be removable or non-migrating, thus preventing contamination of the packaged product with harmful substances.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Ease of operation

If silicone oil is added to reduce removal torque, then ease of operation is improved, but barrier performance deteriorates

Engineering Contradiction:
Improveremoval torqueVSAvoidoxygen barrier performance
Core Design Contradiction:
Ease of operationVSReliability

Solution Approach 1:

The patent modifies the chemical and physical parameters of the sealing element by incorporating specific biorenewable processing aids with controlled molecular weights, viscosity ranges, and polarity characteristics. These parameter adjustments allow the material to achieve appropriate removal torque without compromising oxygen barrier performance, as the biorenewable aids do not interfere with the barrier properties of the polymer matrix like silicone oil does.

Inventive Principle:
Principle #35Parameter changes

3Reliability

If high molecular weight polyisobutylene is used to improve barrier properties, then oxygen barrier performance is improved, but viscosity increases making processing difficult

Engineering Contradiction:
Improveoxygen barrier performanceVSAvoidviscosity
Core Design Contradiction:
ReliabilityVSEase of manufacture

Solution Approach 1:

The biorenewable processing aids serve as intermediary substances that temporarily reduce the viscosity of high molecular weight polyisobutylene during processing. These processing aids interact with the polymer chains to decrease intermolecular friction, enabling easy extrusion and molding. After processing, the processing aids can be removed or become inactive, leaving the high molecular weight polyisobutylene to provide its full oxygen barrier performance without the viscosity penalty.

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The composition achieves significant reductions in oxygen permeability and viscosity, maintaining integrity and ease of processing, while being resistant to high temperatures and suitable for food contact applications.

Implementation Method 1

the biorenewable processing aid acts as a barrier synergist... Low oxygen permeability sealing elements can be formed from the compositions

Methodology Applied
Scientific EffectPermeation: Permeation

Implementation Method 2

achieving desirable oxygen barrier properties without contributing to the taste or odor of packaged products, while also being easily processable

Methodology Applied
Scientific EffectViscosity reduction:

Implementation Method 3

maintaining integrity and ease of processing, while being resistant to high temperatures

Methodology Applied
Scientific EffectThermal resistance: Thermal Insulation

Data Source

PatentEP3212531B1Sealing element compositions having biorenewable content
Publication Date: 2020.12.23 TEKNOR APEX COMPANY
  • EP3212531B1 patent drawingFigure 1~4
  • EP3212531B1 patent drawingFigure 2~3
  • EP3212531B1 patent drawing

AI summary

Thermoplastic elastomer compositions, in particular derived from one or more styrenic block copolymers, a relatively high molecular weight isobutylene-containing (co)polymer, and a biorenewable processing aid. The isobutylene-containing (co)polymer imparts desirable oxygen barrier performance to the composition and the biorenewable processing aid acts as a barrier synergist as well as a processing aid useful during compounding. Low oxygen permeability sealing elements can be formed from the compositions. Processes for preparing the compositions and sealing elements are disclosed.