Rheological Bonding Assessment for Bitumen-Aggregate Mixtures

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Solution Overview

Problem

Assessing changes in bonding interactions between inclusions and a thermoplastic matrix, such as bitumen and stone aggregates, is challenging due to difficulties in repeatability and sample preparation in existing tests.

Innovation Solution

A method involving the preparation of heterogeneous mixtures, subjecting them to ramping shear rates, and assessing viscosity using a power-law equation to determine the slope of the shear-thinning region, which identifies changes in bond strength and susceptibility to conditioning factors like moisture damage.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If traditional tests on stone aggregate, loose mixtures, compacted mixtures, or asphalt binder alone are used, then bonding interaction assessment is performed, but repeatability and sample preparation become difficult

Engineering Contradiction:
Improvebonding interaction assessmentVSAvoidrepeatability
Core Design Contradiction:
Measurement precisionVSReliability

Solution Approach 1:

The patent changes the measurement parameter from traditional mechanical tests to viscosity measurement under controlled shear rates. By measuring viscosity at multiple shear rates and analyzing the shear-thinning region slope, the method achieves consistent, repeatable results that directly reflect bonding interactions between bitumen and aggregates without the variability of traditional preparation methods.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent replaces complex mechanical testing systems (requiring sample preparation, compaction, and mechanical loading) with a rheological measurement system. The viscosity measurement apparatus applies controlled shear rates and measures resistance to flow, substituting mechanical strength tests with fluid mechanics-based viscosity assessment that is more repeatable and easier to standardize.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

2Measurement precision

If traditional bonding interaction tests are performed, then bond strength assessment is obtained, but sample preparation complexity increases

Engineering Contradiction:
Improvebond strength assessmentVSAvoidsample preparation
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The patent extracts the essential bonding interaction information from complex composite samples by measuring viscosity of the bitumen-aggregate mixture directly. Instead of preparing separate aggregate samples, binder samples, or compacted mixtures, the method takes the heterogeneous mixture as-is and measures its rheological properties, eliminating the need for complex sample preparation while retaining bond strength assessment capability.

Inventive Principle:
Principle #2Taking out (Extraction)

3Measurement precision

If viscosity is measured at multiple shear rates, then bonding interaction changes are detected, but test time increases

Engineering Contradiction:
Improvebonding interaction detectionVSAvoidtest time
Core Design Contradiction:
Measurement precisionVSLoss of time

Solution Approach 1:

The patent measures viscosity at multiple shear rates (excessive action) to fully characterize the shear-thinning behavior and accurately determine the slope of the shear-thinning region. This comprehensive approach ensures reliable detection of bonding interaction changes, with the time investment justified by the significant improvement in measurement precision and reliability compared to single-shear-rate tests.

Inventive Principle:
Principle #16Partial or excessive action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach allows for the evaluation of bond strength changes and moisture susceptibility, enabling effective screening of bitumens and additives, and detecting non-durable combinations prone to moisture damage with low coefficients of variation.

Implementation Method 1

assessing a value of a slope of a shear-thinning region for the unconditioned sample using a power-law equation

Methodology Applied
Scientific EffectShear thinning: Shear Thinning

Data Source

PatentUS11761869B2Evaluating changes in bonding interactions between inclusions and a thermoplastic matrix
Publication Date: 2023.09.19 THE ARIZONA BOARD OF REGENTS ON BEHALF OF THE UNIV OF ARIZONA
  • US11761869B2 patent drawing

AI summary

Assessing an interaction between solid particles and a thermoplastic material in which the solid particles are dispersed includes combining a thermoplastic material with a multiplicity of solid particles to yield a heterogeneous mixture, processing the heterogeneous mixture to yield an unconditioned sample, conditioning the unconditioned sample to yield a conditioned sample, subjecting the conditioned sample to a ramping shear rate from an initial shear rate to a final shear rate, assessing a viscosity of the conditioned sample at a plurality of shear rates between the initial shear rate and the final shear rate, and assessing a value of a slope of a shear-thinning region for the unconditioned sample using a power-law equation.