Bonded Diamond Assembly Void Reduction

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Solution Overview

Problem

The challenge lies in bonding large areas of polycrystalline diamond to a substrate while minimizing voids and thermal/barrier resistance, as existing methods face issues with delamination, stress, and reduced power density due to thermal mismatch and uneven bonding.

Innovation Solution

A bonded diamond assembly with a polycrystalline diamond wafer and a substrate bonded using a controlled bonding layer, where ultrasound inspection ensures minimal voids and particulate impurities, and elevated pressure and temperature are applied to enhance bonding, allowing for higher current densities and mechanical load resistance.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Area of stationary object

If large area polycrystalline diamond is bonded to a substrate, then the working surface area is maximized, but voids and defects increase degrading electrode performance

Engineering Contradiction:
Improvebonded areaVSAvoidelectrode performance
Core Design Contradiction:
Area of stationary objectVSReliability

Solution Approach 1:

The patent changes the physical state and parameters of the bonding material by heating it to its melting point and above, transforming it from a viscous paste into a fluid that can flow and fill voids. This parameter change allows the bonding material to adapt to surface irregularities and eliminate defects while bonding large areas.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The bonding material undergoes phase transition from solid/viscous state to liquid/molten state during the bonding process. By heating the bonding material above its melting point, it transitions to a fluid phase that can flow into voids and ensure complete contact between diamond and substrate, then solidifies to form a strong bond.

Inventive Principle:
Principle #36Phase transitions

2Reliability

If viscous electrically conducting epoxy paste is used for bonding, then electrical connection is achieved, but uneven application and poor adhesive flow cause voids

Engineering Contradiction:
Improveelectrical connectionVSAvoidbonding uniformity
Core Design Contradiction:
ReliabilityVSManufacturing precision

Solution Approach 1:

The patent changes the temperature parameter of the bonding material from room temperature to above its melting point during bonding. This parameter change transforms the material from a viscous state with poor flow characteristics into a fluid state that exhibits excellent flow and wetting properties, eliminating voids and ensuring uniform bonding.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The bonding material acts as an intermediary substance that facilitates the connection between diamond and substrate. By controlling its temperature and phase, it mediates the bonding process to achieve both electrical conductivity and void-free bonding uniformity.

Inventive Principle:
Principle #24Intermediary (Mediator)

3Reliability

If diamond layer thickness is limited to reduce stress, then delamination is reduced, but the process becomes commercially less attractive

Engineering Contradiction:
Improvedelamination resistanceVSAvoidcommercial viability
Core Design Contradiction:
ReliabilityVSProductivity

Solution Approach 1:

The bonding material undergoes phase transition to a molten state during bonding, creating a fluid that can flow and fill all interfacial voids and irregularities. This ensures complete wetting and adhesion between diamond and substrate, preventing delamination even in thicker layers without compromising commercial viability.

Inventive Principle:
Principle #36Phase transitions

Solution Approach 2:

By changing the temperature parameter during bonding to above the melting point of the bonding material, the patent achieves superior adhesion that allows thicker diamond layers to be bonded without delamination, maintaining both reliability and commercial attractiveness.

Inventive Principle:
Principle #35Parameter changes

4Quantity of substance

If thicker diamond layers are produced, then more material is available for application, but production cost increases proportionally

Engineering Contradiction:
Improvediamond layer thicknessVSAvoidproduction cost
Core Design Contradiction:
Quantity of substanceVSEase of manufacture

Solution Approach 1:

The bonding material transitions to a molten state during bonding, creating a fluid that flows and fills all interfacial voids and irregularities. This ensures complete wetting and adhesion between diamond and substrate, preventing delamination even in thicker layers without compromising commercial viability.

Inventive Principle:
Principle #36Phase transitions

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution effectively bonds larger diamond areas with low thermal and electrical resistivity, reducing void-related issues and maintaining performance across varying temperatures, enabling higher current densities and mechanical stability.

Implementation Method 1

a bonding layer located between the diamond and the substrate and bonding them together

Methodology Applied
Scientific EffectAdhesion: Adhesive

Implementation Method 2

The bonding layer, when inspected using ultrasound using a resolution of 50 μm, a focal length selected to inspect the bonding layer, and frequencies of 100 MHz and 30 MHz

Methodology Applied
Scientific EffectUltrasound: Ultrasound

Implementation Method 3

elevated pressure and temperature are applied to enhance bonding

Methodology Applied
Scientific EffectPressure: Pressure Increase

Implementation Method 4

elevated pressure and temperature are applied to enhance bonding

Methodology Applied
Scientific EffectThermal energy: Heating

Implementation Method 5

low electrical resistivity while retaining an acceptable amount of voids and particulate impurities in the bonding layer

Methodology Applied
Scientific EffectElectrical conduction: Conduction (electrical)

Implementation Method 6

low thermal barrier resistance

Methodology Applied
Scientific EffectThermal conduction: Conduction (thermal)

Data Source

PatentUS20230406732A1A diamond assembly
Publication Date: 2023.12.21 ELEMENT SIX TECH LTD
  • US20230406732A1 patent drawing
  • US20230406732A1 patent drawing
  • US20230406732A1 patent drawing

AI summary

A bonded diamond assembly and a method of forming the assembly. The assembly comprises a polycrystalline diamond wafer having a largest linear dimension of between 25 mm and 200 mm, a substrate and a bonding layer located between the diamond and the substrate and bonding them together. The bonding layer, when inspected using ultrasound using a resolution of 50 μm, a focal length selected to inspect the bonding layer, and frequencies of 100 MHz and 30 MHz, comprises low numbers of voids extending either across the thickness of the bonding layer and low numbers of voids that do not extend across the thickness of the bonding layer.