Borate Crosslinker for Hydraulic Fracturing Fluids

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Solution Overview

Problem

Hydraulic fracturing processes face challenges in efficiently delivering proppants due to high viscosity carrier fluids, which increase friction pressure and limit fracture width and length, while existing crosslinking agents lack flexibility in controlling the crosslinking rate to match the timing of pumping and delivery processes.

Innovation Solution

A crosslinking composition comprising a balance of hydroboracite and borax, optimized with additives like canola oil, xanthan, and glycerol, allows for customizable crosslinking rates, maintaining lower viscosity during pumping to reduce friction and achieving higher viscosity upon delivery, thereby enhancing proppant delivery and fracture stability.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If higher viscosity carrier fluids are used to carry proppants more effectively, then proppant delivery effectiveness is enhanced, but friction pressure within pumps increases

Engineering Contradiction:
Improveproppant delivery effectivenessVSAvoidfriction pressure
Core Design Contradiction:
ProductivityVSStress or pressure

Solution Approach 1:

The patent applies dynamic viscosity control by using crosslinking agents that adjust the fluid's viscosity over time. The carrier fluid starts with lower viscosity for easy pumping, then progressively increases viscosity through crosslinking reactions during transport, optimizing both pumpability and proppant carrying capacity at different stages of the process.

Inventive Principle:
Principle #15Dynamics

Solution Approach 2:

The crosslinking agents are pre-added to the carrier fluid before pumping begins, initiating a controlled viscosity increase that progresses during transport. This preliminary action allows the fluid to automatically adapt its viscosity characteristics to match the changing requirements from pumping to proppant delivery.

Inventive Principle:
Principle #10Preliminary action

2Length of stationary object

If higher viscosity fluids are used to carry higher concentrations of proppant, then fracture width is enabled to increase, but friction pressure in the system increases

Engineering Contradiction:
Improvefracture widthVSAvoidfriction pressure
Core Design Contradiction:
Length of stationary objectVSStress or pressure

Solution Approach 1:

The fluid viscosity dynamically evolves from a pumpable state to a high-viscosity gel state during transport. This time-dependent viscosity change allows the system to achieve high fracture width capability at the destination while maintaining acceptable pumping pressures during transport.

Inventive Principle:
Principle #15Dynamics

3Adaptability or versatility

If existing crosslinking agents are used, then crosslinking can occur, but flexibility in controlling the crosslinking rate to match pumping and delivery timing is limited

Engineering Contradiction:
Improvecrosslinking rate control flexibilityVSAvoidtiming mismatch
Core Design Contradiction:
Adaptability or versatilityVSLoss of time

Solution Approach 1:

The patent introduces multiple crosslinking agents with different reaction rates and mechanisms. By selecting and combining agents with specific kinetic properties, the system can precisely control the timing and rate of viscosity development to match various pumping and delivery schedules, eliminating timing mismatches.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The composition uses composite crosslinking systems combining multiple agents (e.g., borax, boric acid, zinc chloride) that work synergistically. This composite approach provides broader control over crosslinking kinetics, allowing customization of the viscosity development profile to match specific operational requirements.

Inventive Principle:
Principle #40Composite materials

4Speed

If crosslinking occurs too quickly after mixing, then high viscosity is achieved rapidly, but the fluid may not be deliverable to fractures in time

Engineering Contradiction:
Improvecrosslinking speedVSAvoiddelivery delay
Core Design Contradiction:
SpeedVSLoss of time

Solution Approach 1:

The crosslinking process is designed to be dynamic and controllable, progressing at a rate that can be matched to the pumping and delivery schedule. The fluid transitions from a low-viscosity pumpable state to a high-viscosity deliverable state over a controlled time period, ensuring availability at the fracture destination.

Inventive Principle:
Principle #15Dynamics

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution enables efficient proppant delivery with reduced friction pressure and increased fracture width and length, while allowing for tailored crosslinking timing to match hydraulic fracturing operations, improving the overall effectiveness of the fracturing process.

Implementation Method 1

customizable crosslinking rates... as the balance between hydroboracite and borax favors hydroboracite, the rate at which the composition crosslinks guar will decrease. Likewise, as the balance favors borax, the rate at which the composition crosslinks guar or HPG will increase.

Methodology Applied
Scientific EffectIon release: Diffusion

Implementation Method 2

Crosslinking hydrated guar suspensions, or suspensions of various guar derivatives, can create a gel fluid with relatively high viscosity.

Methodology Applied
Scientific EffectCrosslinking: Chemical Bonding

Implementation Method 3

a thickening or stabilizing agent such as xanthan or a similar rheology modifier, and a polyol such as glycerol

Methodology Applied
Scientific EffectRheology modification: Non-Newtonian Fluids

Data Source

PatentUS10358594B2Borate crosslinker
Publication Date: 2019.07.23 PFP TECH LLC

AI summary

The present disclosure relates to a crosslinking composition for use in crosslinking an aqueous suspension of guar, for use as a well treatment fluid and/or proppant carrier fluid for natural gas extraction. The present crosslinking composition is an aqueous suspension of hydroboracite. The composition may also comprise varying amounts of borax, canola oil, xanthan, glycerol, and/or NaOH. The composition may be selected to effect a desired delay in the crosslinking reaction in order to customize the viscosity and reaction time to the method of use, thereby maximizing proppant delivery while minimizing pump pressure.