Boric Acid Crystal Separation in Nuclear Waste Evaporation

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Solution Overview

Problem

The disposal of boric acid-water mixtures from pressurized water reactors poses environmental and safety challenges due to radioactive contamination, requiring an environmentally friendly, economical, and safe treatment method.

Innovation Solution

A system utilizing a vacuum evaporator and separator to concentrate and separate boric acid crystals from the mixture, with a two-stage evaporation process and subsequent drying, allowing for the separation of radioactively cleaned fractions that can be reused or stored as ordinary waste.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If boric acid-water mixture is concentrated by evaporation, then boric acid crystals are formed and separated from the mixture, but agglomerates and deposits form on the inner wall of the evaporator

Engineering Contradiction:
Improveconcentration of boric acidVSAvoidagglomerates and deposits on evaporator wall
Core Design Contradiction:
Quantity of substanceVSObject-generated harmful factors

Solution Approach 1:

The system performs preliminary action by dissolving deposited boric acid crystals from the evaporator wall using a dissolving water line before they can form harmful agglomerates. This preventive measure is taken during the evaporation process to maintain clean evaporator surfaces and ensure efficient heat transfer throughout the concentration cycle.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

Dissolving water acts as an intermediary substance that facilitates the removal of deposited boric acid crystals from the evaporator wall. This intermediary fluid dissolves the deposits and transports them away, preventing the formation of harmful agglomerates without interfering with the main evaporation process.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Ease of manufacture

If boric acid-water mixture is discharged into water body in diluted form, then disposal is simple and economical, but environmental protection requirements are violated

Engineering Contradiction:
Improvedisposal simplicity and costVSAvoidenvironmental contamination
Core Design Contradiction:
Ease of manufactureVSObject-affected harmful factors

Solution Approach 1:

The system segments the boric acid-water mixture into two distinct fractions through evaporation and separation: a concentrated boric acid crystal fraction and a water fraction. This segmentation allows each fraction to be disposed of or reused according to its specific characteristics, with the water fraction being safe for environmental discharge and the crystal fraction requiring specialized handling.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The system changes the concentration parameter of the boric acid-water mixture through controlled evaporation. By adjusting the water content and achieving different concentration levels, the mixture is transformed from a diluted state suitable for environmental discharge to a concentrated state where crystals form and can be separated for appropriate disposal or reuse.

Inventive Principle:
Principle #35Parameter changes

3Quantity of substance

If mother liquor is returned to evaporator for reprocessing, then radioactivity is concentrated in fewer fractions, but energy consumption increases

Engineering Contradiction:
Improveradioactivity concentration in waste fractionVSAvoidenergy consumption of evaporator
Core Design Contradiction:
Quantity of substanceVSUse of energy by moving object

Solution Approach 1:

The system implements feedback by measuring the radioactivity level of the mother liquor and using this information to control the reprocessing decision. A radiation detector monitors the radioactivity concentration, and based on these measurements, the system determines whether the mother liquor should be returned to the evaporator for further concentration or disposed of through alternative routes, optimizing energy usage while ensuring safe radioactivity management.

Inventive Principle:
Principle #23Feedback

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This method effectively reduces radioactivity in the boric acid crystals, enabling their safe storage or reuse, with no secondary waste and low operational costs, while preventing agglomerate formation in the evaporator and dryer.

Implementation Method 1

the boric acid-water mixture is concentrated by partially evaporating the water in a vacuum evaporator

Methodology Applied
Scientific EffectEvaporation: Evaporation

Implementation Method 2

This suspension is separated into the mother liquor and the crystals in a downstream separator

Methodology Applied
Scientific EffectCentrifugal separation: Centrifugal Separation

Data Source

PatentEP3955264A1System and method for separating boric acid crystals from a boric acid-water mixture
Publication Date: 2022.02.16 ENBW ENERGIE BADEN WURTTEMBERG AG
  • EP3955264A1 patent drawingFigure 1
  • EP3955264A1 patent drawingFigure 2
  • EP3955264A1 patent drawingFigure 3

AI summary

A system and process for separating and processing boric acid from a boric acid-water mixture are proposed. The invention is highly effective, requires no auxiliary materials, and produces no secondary waste. Furthermore, it is easily automated and safe to operate. The system is used for the treatment of radioactive materials/contamination and is suitable for operation in the controlled area of ​​a nuclear facility.