Borinic Ester Stabilization in Oral Care via pH Buffering

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Solution Overview

Problem

Borinic esters are unstable and insoluble in aqueous compositions, making them challenging to incorporate effectively into oral care products like dentifrice for antimicrobial purposes, as they hydrolyze and decompose, and have limited solubility in water and oils.

Innovation Solution

Stabilizing borinic esters by maintaining a pH above 7, using buffering agents, and incorporating them with solubilizing agents such as polyoxyethylene and polyoxypropylene polymers, which enhances their solubility and antimicrobial activity in oral care compositions.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If borinic esters are incorporated into aqueous oral care compositions, then antimicrobial activity is achieved, but stability deteriorates due to hydrolysis and decomposition

Engineering Contradiction:
Improveantimicrobial activityVSAvoidchemical stability
Core Design Contradiction:
ReliabilityVSStability of the object's composition

Solution Approach 1:

The patent employs buffering agents as intermediary substances that mediate between the borinic ester and the aqueous environment. The buffer system (maintaining pH 7 or higher) acts as a protective intermediary that prevents direct hydrolytic attack on the borinic ester, thereby preserving its chemical stability while allowing it to remain in the aqueous oral care composition and exert its antimicrobial effect

Inventive Principle:
Principle #24Intermediary (Mediator)

2Reliability

If borinic esters are added to aqueous compositions, then antimicrobial function is provided, but solubility worsens due to limited water and oil solubility

Engineering Contradiction:
Improveantimicrobial functionVSAvoidsolubility
Core Design Contradiction:
ReliabilityVSQuantity of substance

Solution Approach 1:

The patent applies parameter changes by modifying the pH parameter of the aqueous composition (maintaining pH at 7 or higher) to enhance the solubility of borinic esters. This parameter change prevents the ester from precipitating or separating, allowing sufficient quantity to remain dissolved in the aqueous oral care composition while maintaining its antimicrobial function

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The approach results in stable, soluble, and effective antimicrobial borinic esters that can be used in oral care products to reduce bacteria, inhibit plaque, and treat dental caries and gingivitis, maintaining their antimicrobial activity and stability over time.

Implementation Method 1

Stabilizing borinic esters by maintaining a pH above 7, using buffering agents

Methodology Applied
Scientific EffectpH buffering:

Implementation Method 2

incorporating them with solubilizing agents such as polyoxyethylene and polyoxypropylene polymers, which enhances their solubility

Methodology Applied
Scientific EffectSolubilization: Solvation

Data Source

PatentEP2437854B1Compositions comprising borinic esters
Publication Date: 2018.08.08 COLGATE PALMOLIVE CO
  • EP2437854B1 patent drawingFigure 1(a)~1(b)
  • EP2437854B1 patent drawingFigure 2
  • EP2437854B1 patent drawing

AI summary

A stabilized oral care composition comprising a borinic acid derivative, e.g., a borinic ester.