Boron Nitride Nano-Onion Synthesis via Lamp Ablation

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Solution Overview

Problem

Current methods for producing boron nitride nanostructures are complex, inefficient, and often require toxic chemicals, making them difficult to scale and environmentally unfriendly, with limited success in producing nano-onion structures.

Innovation Solution

Subjecting boron nitride precursor material to lamp ablation within an adiabatic radiative shielding environment, such as a hermetically sealed fused quartz vessel, to produce a variety of nanostructures including nano-onions, which are crystalline and have high purity and yield.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If conventional methods (pulsed laser ablation, chemical vapour deposition, electron beam irradiation, pyrolysis) are used to produce boron nitride nanostructures, then nanostructures can be obtained, but the production process becomes complex requiring multiple steps, catalysts, templates, and/or complex facilities

Engineering Contradiction:
Improveproduction of boron nitride nanostructuresVSAvoidcomplexity of production process
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent extracts and eliminates the need for catalysts, templates, and multiple processing steps from the conventional production methods. By using lamp ablation of boron nitride precursor material in a simple apparatus, the invention removes the disturbing elements (catalysts, templates, complex facilities) while maintaining the ability to produce boron nitride nanostructures including nano-onions

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent replaces complex mechanical and chemical systems (multiple steps, catalysts, templates) with a simplified optical/thermal system (lamp ablation). The lamp provides concentrated light energy that directly converts precursor material into nanostructures through ablation, eliminating the need for complex mechanical processing and chemical catalysis

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

2Reliability

If chemical synthetic techniques are used to produce boron nitride nanostructures, then nanostructures can be obtained, but the product yield and purity are poor and toxic chemicals such as NaN3 are employed

Engineering Contradiction:
Improveproduction of boron nitride nanostructuresVSAvoidtoxic chemicals and poor product quality
Core Design Contradiction:
ReliabilityVSObject-generated harmful factors

Solution Approach 1:

The patent converts the harmful chemical synthesis approach into a beneficial physical process. By using lamp ablation instead of chemical synthesis, the invention eliminates toxic chemicals while improving product yield and purity. The high energy light input directly transforms precursor material into high-quality nanostructures without harmful byproducts

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

Solution Approach 2:

The patent changes the fundamental parameters of the synthesis process from chemical reactions to physical ablation. By using concentrated light energy from the lamp to directly convert precursor material into nanostructures, the invention achieves superior product quality and eliminates toxic chemicals associated with chemical synthesis methods

Inventive Principle:
Principle #35Parameter changes

3Reliability

If methods utilising concentrated light energy are used to synthesise boron nitride nanostructures, then synthesis can be achieved, but the set-up is complex and nano-onion structures are not produced

Engineering Contradiction:
Improvesynthesis of boron nitride nanostructuresVSAvoidcomplexity of set-up
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent creates a universal apparatus that can produce multiple types of boron nitride nanostructures (nano-tubes, nano-sheets, nano-onions, etc.) through a single lamp ablation process. The simple apparatus design with a lamp and precursor material holder serves multiple functions, eliminating the need for different complex set-ups for different nanostructure types

Inventive Principle:
Principle #6Universality (Multi-functionality)

4Manufacturing precision

If reported methods are used to produce boron nitride nano-onions, then some nano-onion structures can be obtained, but the manufacturing process is difficult and not scalable

Engineering Contradiction:
Improveproduction of nano-onion structuresVSAvoiddifficulty of manufacturing process
Core Design Contradiction:
Manufacturing precisionVSEase of manufacture

Solution Approach 1:

The lamp ablation process is self-regulating and self-organizing, requiring minimal intervention. The concentrated light energy automatically converts precursor material into nano-onion structures through a self-organizing process, eliminating the need for complex manual operations, precise template placement, or multiple processing steps. This makes the process both precise and easily scalable

Inventive Principle:
Principle #25Self-service

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This method is simple, scalable, and environmentally friendly, producing a high proportion of crystalline boron nitride nano-onion structures with high purity, suitable for applications as lubricants and anti-wear materials.

Implementation Method 1

Lamp ablation uses high flux bright light to irradiate precursor materials to achieve reactions that are not attainable in conventional ovens or alternative pathways.

Methodology Applied
Scientific EffectLamp ablation: Laser Ablation

Implementation Method 2

subjecting boron nitride precursor material to lamp ablation within an adiabatic radiative shielding environment

Methodology Applied
Scientific EffectAdiabatic heating: Adiabatic Heating

Data Source

PatentUS12060267B2Boron nitride nanostructures
Publication Date: 2024.08.13 ONALBA PTY LTD
  • US12060267B2 patent drawing
  • US12060267B2 patent drawing
  • US12060267B2 patent drawing

AI summary

The present invention relates to a method for producing boron nitride nanostructures, the method comprising subjecting boron nitride precursor material to lamp ablation within an adiabatic radiative shielding environment. The nanostructures produced may include nano-onion structures. The boron nitride precursor material subjected to lamp ablation may include amorphous boron nitride, hexagonal boron nitride, cubic boron nitride, wurtzite boron nitride or a combination of two or more thereof.