Boron Oxide FCC Catalysts for Resid Cracking

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Solution Overview

Problem

Current fluid catalytic cracking (FCC) catalysts face challenges in minimizing coke and hydrogen yields, especially when processing resid feeds containing high levels of contaminant metals like nickel and vanadium, which lead to decreased gasoline production and increased operational costs due to heat imbalance and compressor expenses.

Innovation Solution

Incorporating FCC compatible inorganic particles containing one or more boron oxide components into the catalyst composition to reduce coke and hydrogen yields by passivating deleterious metals, thereby maintaining catalyst selectivity and stability.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If conventional FCC catalysts are used to process resid feeds, then cracking activity is maintained, but coke and hydrogen yields increase due to metal contaminants

Engineering Contradiction:
Improvecracking activityVSAvoidcoke and hydrogen yields
Core Design Contradiction:
ProductivityVSObject-generated harmful factors

Solution Approach 1:

Boron oxide serves as an intermediary substance that selectively interacts with contaminant metals (Ni, V, Fe) to form stable borates, preventing these metals from catalyzing unwanted dehydrogenation reactions. The boron oxide acts as a passivating agent that mediates between the harmful metals and the hydrocarbon feed, eliminating their detrimental effects on coke and hydrogen formation while preserving zeolite cracking activity

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The invention converts the harmful effect of metal contaminants into a beneficial outcome by using boron oxide to selectively trap these metals. The metals that would normally increase coke and hydrogen yields are instead captured by boron oxide to form stable borates, transforming a harmful catalytic effect into a beneficial passivation mechanism that protects the zeolite from metal-induced deactivation

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

2Productivity

If catalyst activity is increased to improve gasoline yield, then conversion efficiency improves, but selectivity decreases with higher coke and gas production

Engineering Contradiction:
Improvegasoline yieldVSAvoidcatalyst selectivity
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The catalyst composition exhibits local quality differentiation where boron oxide is strategically positioned to provide selective passivation at metal contamination sites, while the zeolite maintains its inherent gasoline-selective cracking activity in uncontaminated regions. This spatial differentiation of functions allows high activity and high selectivity to coexist by localizing the protective effect where metals are present

Inventive Principle:
Principle #3Local quality

3Productivity

If resid feeds are processed to maximize heavy hydrocarbon conversion, then feed utilization improves, but contaminant metal effects increase coke and hydrogen formation

Engineering Contradiction:
Improvefeed conversion efficiencyVSAvoidcoke and hydrogen from metal contaminants
Core Design Contradiction:
ProductivityVSObject-generated harmful factors

Solution Approach 1:

Boron oxide is incorporated into the catalyst composition in advance to provide preliminary protection against metal contaminants before they can cause harm. The boron oxide is pre-positioned on the catalyst surface to intercept and passivate metals as they are introduced with the resid feed, preventing the subsequent formation of unwanted coke and hydrogen that would occur without this preliminary protective action

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The use of boron oxide components in the FCC catalyst composition effectively lowers hydrogen and coke yields, enhancing gasoline production and reducing operational costs by preventing metal-induced dehydrogenation reactions and maintaining catalyst performance under varying hydrocarbon feed conditions.

Implementation Method 1

Incorporating FCC compatible inorganic particles containing one or more boron oxide components into the catalyst composition to reduce coke and hydrogen yields by passivating deleterious metals

Methodology Applied
Scientific EffectPassivation: Adsorption

Implementation Method 2

Catalytic cracking in current FCC catalysts is attributable to both the zeolite and non-zeolite (e.g. matrix) components

Methodology Applied
Scientific EffectCatalysis: Catalysis

Data Source

PatentUS10525451B2FCC catalyst compositions containing boron oxide
Publication Date: 2020.01.07 BASF CORPORATON

AI summary

Described are fluid catalytic cracking (FCC) compositions, methods of manufacture and use. FCC catalyst compositions comprise particles containing a non-zeolitic component and one or more boron oxide components. In embodiments, the FCC catalyst composition contains a zeolite component and optionally a rare earth component and a transition alumina. FCC catalytic compositions may comprise a first particle type containing one or more boron oxide components and a first matrix component mixed with a second particle type containing a second matrix component, and a zeolite. The FCC catalyst compositions can be used to crack hydrocarbon feeds, particularly resid feeds containing high V and Ni, resulting in lower hydrogen and coke yields.