Carbon-Carbon Brake Disk Micro-Crack Sealing by Final CVD

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Solution Overview

Problem

The manufacturing process of carbon/carbon brake disks often results in micro-cracks due to final heat treatment, which allows moisture and oxidation protection systems to penetrate, leading to reduced friction performance and wear life.

Innovation Solution

A method involving the formation of a fibrous network from oxidized carbon fibers, carbonization, infiltration with carbon using CVI/CVD processing, and a final chemical vapor deposition (CVD) process at 1000°C to fill micro-cracks and prevent penetration of oxygen, moisture, and oxidation protection systems.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Strength

If final heat treatment (FHT) process is performed at high temperature (1400-2200°C), then mechanical strength and friction performance are improved, but micro-cracks are generated in the C/C part

Engineering Contradiction:
Improvemechanical strengthVSAvoidmicro-crack formation
Core Design Contradiction:
StrengthVSManufacturing precision

Solution Approach 1:

The patent performs a preliminary action by conducting a final chemical vapor deposition (CVD) process at approximately 1000°C after the high-temperature FHT process. This secondary CVD process deposits carbon material that fills the micro-cracks generated during FHT, sealing them before the brake disk enters service. The low-temperature CVD treatment is applied in advance to prevent harmful effects of micro-cracks while maintaining the mechanical strength benefits of high-temperature FHT.

Inventive Principle:
Principle #10Preliminary action

2Productivity

If micro-cracks are present in the C/C part, then manufacturing complexity is reduced, but penetration of oxygen, moisture, and OPS chemicals occurs leading to reduced wear life

Engineering Contradiction:
Improvemanufacturing efficiencyVSAvoidwear life
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The patent converts the harmful effect of micro-cracks into a beneficial process by utilizing them as pathways for carbon deposition. During the final CVD process at 1000°C, carbon material deposits preferentially into the micro-cracks, filling them and transforming these defects into sealed, structurally sound regions. This approach maintains manufacturing efficiency while eliminating the reliability issues caused by micro-crack penetration of oxygen, moisture, and OPS chemicals.

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

3Manufacturing precision

If final CVD process is performed for extended duration (20-100 hours), then micro-crack filling and seal quality are improved, but manufacturing time and energy consumption increase

Engineering Contradiction:
Improvemicro-crack filling qualityVSAvoidprocessing time
Core Design Contradiction:
Manufacturing precisionVSLoss of time

Solution Approach 1:

The patent optimizes the balance between micro-crack filling quality and processing time by carefully controlling CVD parameters including temperature (approximately 1000°C), pressure, carbon source gas composition, and deposition time (20-100 hours). By adjusting these parameters, the process achieves adequate micro-crack sealing without requiring excessively long processing times, thereby reducing energy consumption and manufacturing cycle time while maintaining sufficient seal quality.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method increases the wear life of carbon/carbon brake disks by sealing micro-cracks and preventing inhibitors from reaching the wear surface, thereby maintaining friction performance and mechanical strength.

Implementation Method 1

performing a final chemical vapor deposition (CVD) process at approximately 1000° C. to at least partially fill in a micro-crack in the C/C part

Methodology Applied
Scientific EffectChemical vapor deposition: Chemical Vapour Deposition

Implementation Method 2

carbonizing the oxidized carbon fiber precursor by heating the oxidized carbon fiber precursor at 1400-2800° C. to form a carbon fiber

Methodology Applied
Scientific EffectCarbonization: Pyrolysis

Data Source

PatentUS11396483B2Systems and methods for producing a carbon composite material
Publication Date: 2022.07.26 GOODRICH CORP
  • US11396483B2 patent drawing
  • US11396483B2 patent drawing

AI summary

A carbon/carbon brake disk is provided. The carbon/carbon brake disk may comprise a carbon fiber, wherein the carbon fiber is formed into a fibrous network, wherein the fibrous network comprises carbon deposited therein. The carbon fiber may undergo a FHT process, wherein micro-cracks are disposed in the carbon fiber. In various embodiments, the micro-cracks may be at least partially filled with un-heat-treated carbon via a final CVD process, wherein the final CVD process is performed at a temperature in the range of up to about 1,000° C. (1,832° F.) for a duration in the range from about 20 hours to about 100 hours. In various embodiments, the un-heat-treated carbon may be configured to prevent oxygen, moisture, and/or oxidation protection systems (OPS) chemicals from penetrating the carbon/carbon brake disk. In various embodiments, the final CVI/CVD process may be configured to increase the wear life of the carbon/carbon brake disk.