Branched Polyamic Amide Aerogel for Thermal Stability

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Solution Overview

Problem

Existing polyimide aerogels suffer from brittleness, poor thermal stability, and complex manufacturing processes, limiting their flexibility, mechanical properties, and recyclability.

Innovation Solution

The development of aerogels with a branched polyamic amide polymer within their polymer matrix, which exhibits high branching and little to no crosslinking, enhancing flexibility, thermal stability, and manufacturability.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Temperature

If cross-linked polymer aerogels are used to improve thermal stability, then thermal properties are improved, but flexibility deteriorates and manufacturing complexity increases

Engineering Contradiction:
Improvethermal stabilityVSAvoidflexibility
Core Design Contradiction:
TemperatureVSEase of operation

Solution Approach 1:

The patent changes the chemical structure parameter from cross-linked polyimide to branched polyamic amide polymer. This structural parameter change allows the material to achieve thermal stability through the branched architecture and polyamic amide bonds without requiring cross-linking, thereby maintaining flexibility and reducing manufacturing complexity.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent uses a composite approach by incorporating the branched polyamic amide polymer into the aerogel matrix. This composite structure combines the thermal stability benefits of polyamic amide with the flexibility and processability of aerogel, achieving both thermal performance and mechanical flexibility without cross-linking.

Inventive Principle:
Principle #40Composite materials

2Temperature

If cross-linked polymer aerogels are used to improve thermal stability, then thermal properties are improved, but manufacturing complexity increases

Engineering Contradiction:
Improvethermal stabilityVSAvoidmanufacturing complexity
Core Design Contradiction:
TemperatureVSDevice complexity

Solution Approach 1:

The patent changes the chemical structure parameter from cross-linked polyimide to branched polyamic amide polymer. This structural parameter change allows the material to achieve thermal stability through the branched architecture and polyamic amide bonds without requiring cross-linking, thereby maintaining flexibility and reducing manufacturing complexity.

Inventive Principle:
Principle #35Parameter changes

3Ease of manufacture

If traditional polyimide aerogels are used, then manufacturing process is established, but brittleness and poor thermal stability occur

Engineering Contradiction:
ImprovemanufacturabilityVSAvoidmechanical properties
Core Design Contradiction:
Ease of manufactureVSStrength

Solution Approach 1:

The patent uses a composite approach by incorporating the branched polyamic amide polymer into the aerogel matrix. This composite structure combines the thermal stability benefits of polyamic amide with the flexibility and processability of aerogel, achieving both thermal performance and mechanical flexibility without cross-linking.

Inventive Principle:
Principle #40Composite materials

4Ease of operation

If non-covalently linked compounds are incorporated to improve flexibility, then flexibility is improved, but homogeneity deteriorates and manufacturing difficulty increases

Engineering Contradiction:
ImproveflexibilityVSAvoidhomogeneity
Core Design Contradiction:
Ease of operationVSStability of the object's composition

Solution Approach 1:

The patent changes the chemical structure parameter from cross-linked polyimide to branched polyamic amide polymer. This structural parameter change allows the material to achieve thermal stability through the branched architecture and polyamic amide bonds without requiring cross-linking, thereby maintaining flexibility and reducing manufacturing complexity.

Inventive Principle:
Principle #35Parameter changes

Data Source

PatentEP3408318B1Polymer aerogel with improved mechanical and thermal properties
Publication Date: 2025.04.16 BLUESHIFT MATERIALS INC
  • EP3408318B1 patent drawingFigure 1~2
  • EP3408318B1 patent drawingFigure 3
  • EP3408318B1 patent drawingFigure 4

AI summary

Aerogel compositions that include polyamic amides, methods for preparing the aerogel compositions, and articles of manufacture that include or are manufactured from the aerogel compositions are described.