Branched Polyethylene Rubber Composite for Foamed Seal Strips

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Solution Overview

Problem

Existing foamed rubber materials face challenges in achieving both good heat and aging resistance while maintaining mechanical properties, particularly with the peroxide vulcanization system, which compromises tensile strength and tear strength.

Innovation Solution

A rubber composition incorporating branched polyethylene with a degree of branching of not less than 50 branches/1000 carbon atoms, combined with EPM and EPDM, and utilizing a peroxide-based crosslinking system, along with a low-temperature radiation pre-vulcanization process, to enhance crosslinking efficiency and foaming performance.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If a peroxide vulcanization system is used to achieve excellent heat and aging resistance, then heat resistance and aging resistance are improved, but tensile strength and tear strength are lowered

Engineering Contradiction:
Improveheat and aging resistanceVSAvoidtensile strength and tear strength
Core Design Contradiction:
ReliabilityVSStrength

Solution Approach 1:

The patent combines peroxide vulcanization system with sulfur vulcanization system to create a hybrid crosslinking network. The peroxide provides C-C crosslinks for heat and aging resistance, while sulfur contributes polysulfide bonds for enhanced tensile and tear strength, thus merging the advantages of both systems.

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The invention uses a composite crosslinking structure where peroxide-crosslinked polyethylene forms the base network and sulfur-crosslinked ethylene-propylene rubber segments are integrated into it. This composite material approach allows simultaneous achievement of thermal stability and mechanical strength.

Inventive Principle:
Principle #40Composite materials

2Reliability

If EPM is used to improve aging resistance, then aging resistance is improved, but mechanical strength is lowered

Engineering Contradiction:
Improveaging resistanceVSAvoidmechanical strength
Core Design Contradiction:
ReliabilityVSStrength

Solution Approach 1:

The patent creates a composite rubber composition where EPM segments provide aging resistance through their saturated structure, while EPDM segments contribute to mechanical strength. The peroxide vulcanization system crosslinks both segments into a unified network that exhibits both properties.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

Different regions of the rubber molecule are optimized for different functions: EPM segments with higher saturation are positioned to provide aging resistance, while EPDM segments with pendant groups are optimized for crosslinking and mechanical strength, creating local quality differentiation within the material.

Inventive Principle:
Principle #3Local quality

3Reliability

If degree of branching is increased to improve aging resistance, then aging resistance is improved, but process difficulty and raw material cost increase

Engineering Contradiction:
Improveaging resistanceVSAvoidprocess difficulty and raw material cost
Core Design Contradiction:
ReliabilityVSEase of manufacture

Solution Approach 1:

The patent optimizes the degree of branching parameter to a specific range (50-200 branches per 1000 carbon atoms) that balances aging resistance with processability. This parameter optimization ensures sufficient tertiary carbon atoms for crosslinking while avoiding excessive branching that would complicate processing and increase costs.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution achieves improved aging resistance, mechanical strength, and compression set resistance, while allowing for effective pre-crosslinking control and reduced radiation processing energy, resulting in a foamed rubber product with enhanced performance and productivity.

Implementation Method 1

When a peroxide vulcanization system is used, the foamed material is formed to have single carbon-carbon crosslink bonds

Methodology Applied
Scientific EffectPeroxide vulcanization: Chemical Bonding

Implementation Method 2

When a sulfur vulcanization system is used, the foamed material is formed to have a crosslinked structure mainly composed of polysulfide bonds

Methodology Applied
Scientific EffectSulfur vulcanization: Chemical Bonding

Implementation Method 3

low-temperature radiation pre-vulcanization process, to enhance crosslinking efficiency

Methodology Applied
Scientific EffectRadiation crosslinking: Radiation

Data Source

PatentUS20200123362A1Rubber composite, applications in foamed product, and manufacturing method
Publication Date: 2020.04.23 HANGZHOU XINGLU TECHNOLOGIES CO LTD

AI summary

The present invention discloses a rubber composition, a processing method thereof, and a foamed rubber product produced by the rubber composition and a production method thereof. The rubber composition comprises a rubber matrix and essential components, wherein, based on 100 parts by weight of the rubber matrix, the rubber matrix comprises a branched polyethylene with a content represented as A, in which 0<A≤100 parts; and an EPM and an EPDM with a total content represented as B, in which 0≤B<100 parts, and the essential components comprises 0.5-10 parts of a crosslinking agent, and 1.5-25 parts of a foaming agent. The rubber composition is useful in the production of sponge seal strip, foamed rubber compound of high expansion ratio, shock absorbing foamed rubber sheet, light-colored high-strength foamed sheet, foam-solid composite seal strip, and solid cycle tires internally filled with foamed elastomer. The branched polyethylene replaces a part or all of the ethylene-propylene rubber in the foaming rubber composition, which can increase the melt strength, the foamability and particularly the pre-foamability of the rubber composition, and make the rubber product has a lower compression set.