BrdU Labeled Nucleotide Triphosphates for Non-Isotopic In Situ Hybridization

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

Current in situ hybridization methods, particularly isotopic techniques, are time-consuming and pose safety risks due to the use of radioisotopes, whereas non-isotopic methods lack sensitivity and efficiency in detecting specific DNA or RNA sequences in tissue samples.

Innovation Solution

Development of non-radioactive nucleotide probes, such as 5-bromo-2'-deoxyuridine (BrdU) labeled nucleotides, which are incorporated into polynucleotides and used in conjunction with anti-BrdU antibodies for detection, allowing for sensitive and efficient localization of nucleic acid analytes in tissue samples without the need for radioactive materials.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If isotopic in situ hybridization is used, then detection sensitivity is improved, but safety risks and complexity increase due to radioisotope handling

Engineering Contradiction:
Improvedetection sensitivityVSAvoidsafety risks
Core Design Contradiction:
Measurement precisionVSObject-affected harmful factors

Solution Approach 1:

The patent introduces a non-radioactive intermediary system consisting of BrdU-labeled nucleotides and anti-BrdU antibodies conjugated to detectable moieties (enzymes, fluorophores, or colloidal gold). This intermediary system replaces direct radioactive labeling while maintaining detection sensitivity through the specific antigen-antibody interaction, thereby eliminating safety risks associated with radioisotopes.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Productivity

If non-isotopic in situ hybridization is used, then safety and speed are improved, but detection sensitivity decreases

Engineering Contradiction:
Improveprocedure speedVSAvoiddetection sensitivity
Core Design Contradiction:
ProductivityVSMeasurement precision

Solution Approach 1:

The patent employs parameter changes by modifying the detection system from direct radioactive signal to a multi-component non-radioactive signal amplification system. The anti-BrdU antibody conjugated to enzymes (e.g., alkaline phosphatase) or fluorophores provides enhanced signal intensity, allowing non-isotopic methods to achieve sensitivity comparable to or exceeding isotopic methods while maintaining faster procedure times.

Inventive Principle:
Principle #35Parameter changes

3Productivity

If BrdU labeled probes are used, then safety and procedure time are improved, but manufacturing complexity increases due to multiple components

Engineering Contradiction:
Improveprocedure timeVSAvoidsystem complexity
Core Design Contradiction:
ProductivityVSDevice complexity

Solution Approach 1:

The patent merges multiple functions into integrated components: the anti-BrdU antibody is conjugated directly to detectable moieties (enzymes, fluorophores, or colloidal gold) to create a single reagent that performs both detection and signal generation. This consolidation simplifies the overall system while maintaining the advantages of non-isotopic methods.

Inventive Principle:
Principle #5Merging (Combining)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The BrdU labeled probes provide a safer, quicker, and more sensitive means to detect nucleic acid analytes, avoiding the disadvantages of radioactive isotopes and enabling effective visualization of gene expression in heterogeneous cell populations.

Implementation Method 1

contacting the sample with an anti-BrdU antibody conjugated to a detectable moiety or to an enzyme; and detecting the detectable moiety or enzyme

Methodology Applied
Scientific EffectAntigen-antibody binding:

Data Source

PatentEP2170924B15-bromo-2'-deoxy-uridine labeled nucleotide triphosphates and nucleic acid probes and methods of making and using the same
Publication Date: 2015.07.22 LIFE TECHNOLOGIES CORP
  • EP2170924B1 patent drawingFigure 1
  • EP2170924B1 patent drawingFigure 2
  • EP2170924B1 patent drawing

AI summary

5-bromo-2'-deoxy-uridine (BrdU) labeled nucleotide triphosphates and nucleic acid probes are described herein. The BrdU labeled nucleotide triphosphates include a linker between the nucleotide triphosphate and the BrdU moiety. The linker can be cleavable or non-cleavable. The nucleotide triphosphates can be a ribonucleotide triphosphates, 2'-deoxyribonucleotide triphosphates or 2',3 '-dideoxyribonucleotide triphosphates. The nucleic acid probes can be used for in situ hybridization.