Bubble Column Reactor Bottom Compartment Flushing

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Solution Overview

Problem

Conventional bubble column reactors face issues with sparger plate weeping, leading to potential mechanical damage, disturbed gas distribution, and plugging of the bottom compartment and outlet lines due to reactive material accumulation.

Innovation Solution

Incorporating an inlet and outlet line system for a flushing medium in the bottom compartment, where the medium is continuously introduced and disposed of, preferably transferred downstream of the column reactor, to manage and prevent the consequences of sparger plate weeping.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If a sparger plate is used to divide the column reactor into top and bottom compartments, then gas distribution and reaction efficiency are improved, but weeping occurs leading to mechanical damage and plugging

Engineering Contradiction:
Improvereaction efficiencyVSAvoidmechanical damage and plugging
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

A flushing medium is introduced as an intermediary substance to prevent direct contact between reactive material and the sparger plate. The flushing medium flows through the bottom compartment, dissolving and carrying away reactive material before it can accumulate and cause plugging or mechanical damage, thus protecting the sparger plate while maintaining reaction efficiency

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The invention changes the physical-chemical parameters of the bottom compartment by introducing a flushing medium with different properties. This flushing medium has higher solubility and different reactivity characteristics that prevent the formation of solid deposits and reactive material accumulation, thereby eliminating plugging and mechanical damage while preserving the sparger plate's function

Inventive Principle:
Principle #35Parameter changes

2Device complexity

If the bottom compartment is not flushed, then device complexity is reduced, but reactive material accumulates causing plugging of outlet lines

Engineering Contradiction:
Improvestructure simplicityVSAvoidplugging of outlet lines
Core Design Contradiction:
Device complexityVSEase of operation

Solution Approach 1:

The flushing medium serves multiple functions simultaneously: it protects the sparger plate from mechanical damage, prevents plugging of outlet lines by dissolving reactive material, and maintains gas distribution efficiency. This multi-functionality justifies the addition of the flushing system without proportionally increasing device complexity

Inventive Principle:
Principle #6Universality (Multi-functionality)

Solution Approach 2:

The flushing medium is introduced continuously or periodically to maintain a clean bottom compartment environment. This continuous action prevents the accumulation of reactive material that would otherwise lead to plugging, ensuring uninterrupted operation of the reactor system

Inventive Principle:
Principle #20Continuity of useful action

3Reliability

If flushing medium is continuously introduced into the bottom compartment, then mechanical damage and plugging are prevented, but energy consumption increases

Engineering Contradiction:
Improveprevention of mechanical damage and pluggingVSAvoidenergy consumption
Core Design Contradiction:
ReliabilityVSLoss of energy

Solution Approach 1:

The flushing medium utilizes the existing pressure differential and flow patterns within the reactor system. The flushing action is achieved through the natural flow of the medium through the bottom compartment, leveraging the reactor's own operational characteristics rather than requiring additional energy-intensive pumping or compression systems

Inventive Principle:
Principle #25Self-service

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The continuous flushing of the bottom compartment effectively disposes of materials caused by sparger plate weeping, preventing mechanical damage and plugging, while maintaining efficient gas distribution and processing in the reactor.

Implementation Method 1

By flushing the bottom compartment material (caused by weeping of the sparger plate), being reactive or un-reactive, may be disposed of the bottom compartment

Methodology Applied
Scientific EffectDissolution: Absorption (physical)

Implementation Method 2

Via the bottom compartment a gaseous feed of monomer(s) is introduced into the column reactor and passes through the sparger plate and into the homogenous solution

Methodology Applied
Scientific EffectSparging: Sparging

Data Source

PatentUS8058369B2Method for operating bubble column reactor for the oligomerization of ethylene
Publication Date: 2011.11.15 SAUDI BASIC INDUSTRIES CORP
  • US8058369B2 patent drawing
  • US8058369B2 patent drawing

AI summary

The present invention relates to a bubble column reactor comprising a column reactor having a sparger plate dividing the column reactor into a top reaction compartment and a bottom compartment, characterized in that an inlet and outlet line for introducing and disposing a flushing medium are connected to the bottom compartment; and an operation method thereof.