C-005 Citrate Tablet Dissolution Variability

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Solution Overview

Problem

The pharmaceutical compound C-005 exhibits pH-dependent solubility, leading to variability in absorption due to precipitation in the gastrointestinal tract, causing inconsistent drug absorption rates and amounts between doses and patients, which complicates effective drug delivery and increases safety risks.

Innovation Solution

A pharmaceutical tablet composition is developed with a specific formulation including C-005 citrate, microcrystalline cellulose, crospovidone, and solubilizers like sodium lauryl sulfate, optimized to achieve rapid and complete dissolution within 15-20 minutes at physiologically relevant pH levels, ensuring consistent drug release.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of manufacture

If C-005 is administered as a simple blend in capsule, then the formulation is simple to manufacture, but the dissolution is slow and incomplete leading to high variability in drug absorption

Engineering Contradiction:
Improveformulation simplicityVSAvoiddrug absorption consistency
Core Design Contradiction:
Ease of manufactureVSReliability

Solution Approach 1:

The patent applies preliminary action by pre-forming granules with specific properties before final tablet compression. The granulation process prepares the drug substance in advance with optimized dissolution characteristics, ensuring consistent drug release when the tablet is administered. This pre-preparation of granules with controlled porosity and composition resolves the absorption variability issue while maintaining manufacturing efficiency.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent uses composite materials by combining C-005 with specific excipients including microcrystalline cellulose, crospovidone, and solubilizers in a granulated matrix. This composite formulation enhances dissolution and absorption consistency compared to simple blending, while the granulation process integrates these components into a unified structure that maintains manufacturing simplicity.

Inventive Principle:
Principle #40Composite materials

2Productivity

If the tablet uses high amounts of disintegrant to improve dissolution speed, then the drug release is faster, but the tablet hardness decreases and manufacturing becomes difficult

Engineering Contradiction:
Improvedissolution speedVSAvoidtablet hardness
Core Design Contradiction:
ProductivityVSStrength

Solution Approach 1:

The patent applies parameter changes by optimizing the disintegrant content within a specific range (5-20 wt%) and adjusting granulation parameters such as binder concentration and drying conditions. These parameter optimizations achieve fast dissolution through improved granule porosity and surface area while maintaining adequate tablet hardness for manufacturing, avoiding the need for excessive disintegrant that would compromise structural integrity.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The granulation process performs preliminary action by pre-establishing the porous structure and surface characteristics of the drug matrix before compression. This pre-formed granule structure facilitates rapid drug release upon contact with gastrointestinal fluids while the granules themselves maintain sufficient mechanical strength to form hard tablets during compression.

Inventive Principle:
Principle #10Preliminary action

3Reliability

If the tablet is designed for rapid dissolution to reduce absorption variability, then the drug release is faster and more consistent, but the manufacturing process becomes more complex

Engineering Contradiction:
Improveabsorption consistencyVSAvoidmanufacturing process complexity
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent uses preliminary action through the granulation step that pre-preves the drug matrix with optimized dissolution properties. By performing this preparation in advance, the subsequent compression and coating steps become straightforward, achieving rapid and consistent drug release without requiring complex multi-step manufacturing processes or specialized equipment.

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The tablet composition achieves high and rapid drug release, reducing inter-dose and inter-patient variability in drug absorption, enhancing drug efficacy and safety by maintaining stable drug levels in systemic circulation.

Implementation Method 1

pharmaceutical composition comprising: (a) from 3 to 70 parts by weight of C-005 citrate; (b) from 5 to 95 parts by weight of a pharmaceutical diluent; (c) from 0.5 to 50 parts by weight of a pharmaceutical disintegrant; (d) from 0 to 5 parts by weight of a pharmaceutical solubilizer

Methodology Applied
Scientific EffectSolubilization: Solvation

Data Source

PatentEP3769764B1Pharmaceutical composition and preparation method therefor and uses thereof
Publication Date: 2024.10.30 WUXI SHUANGLIANG BIOTECH CO LTD
  • EP3769764B1 patent drawingFigure 1~2
  • EP3769764B1 patent drawingFigure 3~4
  • EP3769764B1 patent drawingFigure 5~6

AI summary

The present disclosure belongs to the field of pharmaceutical preparations, and discloses a pharmaceutical composition and a preparation method therefor and uses thereof. The pharmaceutical composition comprising EGFR inhibitor (C-005) and the pharmaceutical tablets prepared therefrom of the present disclosure are suitable for the treatment of cancer, preferably lung cancer, particularly non-small cell lung cancer.