Calcium Nitrate Concrete Hydration Control

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Solution Overview

Problem

High ambient temperatures accelerate cement hydration, leading to excessive heat generation, potential cracking, reduced 28-day strength, and surface drying issues in concrete, particularly in hot regions, where existing solutions like retarders may delay setting but also increase drying risks and affect construction progress.

Innovation Solution

Incorporating 3 to 5 weight% calcium nitrate into the cementitious composition to shift hydration reactions to earlier stages, thereby distributing heat release and limiting maximum temperature during curing, especially in temperatures above 27 °C, using calcium nitrate as a setting accelerator.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If quick reacting cements like CEM I 52.5 R are used to accelerate construction progress, then productivity is improved, but temperature increases excessively leading to cracking and reduced 28-day strength

Engineering Contradiction:
Improveconstruction progressVSAvoidmaximum hydration temperature
Core Design Contradiction:
ProductivityVSTemperature

Solution Approach 1:

The invention changes the chemical composition parameters of the cement by incorporating 20-50 wt% slag and 20-50 wt% fly ash to replace Portland cement, fundamentally altering the hydration characteristics and thermal behavior of the cementitious material

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention creates a composite cementitious material combining Portland cement with industrial by-products (slag and fly ash) to achieve both early strength development and controlled heat release, resolving the contradiction between productivity and temperature control

Inventive Principle:
Principle #40Composite materials

2Temperature

If retarders are added to delay setting time and distribute heat release, then temperature control is improved, but setting time is delayed affecting construction progress

Engineering Contradiction:
Improveheat release distributionVSAvoidsetting time
Core Design Contradiction:
TemperatureVSLoss of time

Solution Approach 1:

The invention uses industrial by-products (slag and fly ash) as functional substitutes for expensive chemical retarders, achieving heat release control through material composition rather than chemical admixtures

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

Solution Approach 2:

The invention modifies the chemical composition of the cementitious material to inherently control hydration kinetics, eliminating the need for external retarders that would delay setting time

Inventive Principle:
Principle #35Parameter changes

3Ease of operation

If more mixing water is added to maintain slump in hot conditions, then workability is improved, but 28-day strength decreases significantly

Engineering Contradiction:
ImproveworkabilityVSAvoid28-day compressive strength
Core Design Contradiction:
Ease of operationVSStrength

Solution Approach 1:

The invention changes the chemical composition parameters to include 20-50 wt% slag and 20-50 wt% fly ash, which modify the hydration process to maintain workability without requiring excessive water, thereby preserving strength

Inventive Principle:
Principle #35Parameter changes

4Manufacturing precision

If surface drying is prevented by curing measures in hot conditions, then surface quality is improved, but construction time increases

Engineering Contradiction:
Improvesurface qualityVSAvoidcuring time
Core Design Contradiction:
Manufacturing precisionVSLoss of time

Solution Approach 1:

The invention modifies the chemical composition to include 20-50 wt% slag and 20-50 wt% fly ash, which provide self-curing capabilities through controlled hydration, reducing the need for external curing measures and associated time delays

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach prevents overheating, maintains even heat release, and ensures early strength development without compromising the 28-day strength, while allowing for balanced construction progress in hot conditions, effectively managing temperature peaks and reducing the risk of cracking and surface drying issues.

Implementation Method 1

Hydration is an exothermic reaction, which means that it generates heat, and that reactions proceed faster when the concrete is hot

Methodology Applied
Scientific EffectExothermic reaction: Exothermic Reaction

Implementation Method 2

calcium nitrate is able to shift the maximum heat release to an earlier point of time in the curing process. By this, the hydration energy is distributed over a period of time

Methodology Applied
Scientific EffectHeat release distribution: Exothermic Reaction

Implementation Method 3

when cement hydrates, it takes up water and grows crystals around the aggregate particles

Methodology Applied
Scientific EffectHydration: Mineral Hydration

Data Source

PatentEP2900619B1Process to produce a durable concrete at hot ambient conditions
Publication Date: 2020.11.11 YARA INTERNATIONAL ASA
  • EP2900619B1 patent drawingFigure 1
  • EP2900619B1 patent drawingFigure 2
  • EP2900619B1 patent drawingFigure 3

AI summary

The invention relates to the use of calcium nitrate for producing a cementitious composition and/or a cementitious solid at high ambient temperatures. The invention is directed to ensuring sufficient hydration by a limitation of the maximum hydration temperature.