Capacitive Phase Separator With Dual Probes for High-Pressure Microflows

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Solution Overview

Problem

Current systems fail to effectively separate gases, hydrocarbons, and water in micro-scale laboratory equipment due to size limitations, precision issues, and inability to operate at high pressures, with existing capacitive sensors only capable of separating one liquid phase from a gaseous phase with limited precision.

Innovation Solution

A three-phase capacitive separator device with two electrically isolated probes and RC oscillator circuits that measure capacitance differences to separate gases, hydrocarbons, and water, allowing for controlled outflow and operation at high pressures up to 400 bar, using a tank made of conducting material with a volume between 3 and 20 cm3, and incorporating a refrigeration system for condensation.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If a single capacitive probe is used to separate two phases, then the device structure is simple, but the separation precision and measurement accuracy are limited to 100 μm

Engineering Contradiction:
Improvelevel measurement precisionVSAvoiddevice structure
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The single probe is segmented into two electrically isolated probes, each capable of measuring different phases independently. This segmentation allows for simultaneous measurement of water level and hydrocarbon level with higher precision, while maintaining a relatively simple overall device structure.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The capacitive sensor system is designed to perform multiple functions: separating gases from liquids, separating immiscible liquids (water and hydrocarbons), and providing precise level measurement for each phase. This multi-functionality is achieved through the two-probe configuration that can detect different dielectric materials simultaneously.

Inventive Principle:
Principle #6Universality (Multi-functionality)

2Reliability

If conventional separation systems are used, then they can separate hydrocarbons and water, but they have large system dead volumes and cannot operate at high pressures

Engineering Contradiction:
Improvehigh pressure operation capabilityVSAvoidsystem dead volume
Core Design Contradiction:
ReliabilityVSVolume of stationary object

Solution Approach 1:

The system operates by changing the dielectric parameter (capacitance) to detect and separate different phases. The capacitive sensors measure changes in dielectric constant to identify water, hydrocarbons, and gases, enabling high-pressure operation without mechanical moving parts that would limit pressure capability.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

Mechanical separation systems are replaced with a capacitive sensing system that uses electrical field interactions to detect and separate phases. This substitution eliminates the need for large mechanical separators, allowing the system to operate at high pressures with minimal dead volume.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

3Measurement precision

If gravitational or centrifugal principles are used for separation, then the separation mechanism is simple, but the system cannot achieve precise separation in micro-scale systems

Engineering Contradiction:
Improveseparation precisionVSAvoidseparation mechanism
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

Gravitational and centrifugal mechanical separation mechanisms are replaced with an electrical field-based capacitive sensing system. The system uses differences in dielectric properties to detect and separate phases with high precision in micro-scale volumes, eliminating the need for large-scale mechanical forces.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Solution Approach 2:

The system exploits changes in dielectric parameters to achieve separation. By measuring capacitance variations caused by different materials (water, hydrocarbons, gases), the system achieves precise separation in micro-scale configurations where gravitational and centrifugal forces are insufficient.

Inventive Principle:
Principle #35Parameter changes

4Volume of stationary object

If the tank volume is reduced to 3-20 cm3 for micro-scale applications, then the system dead volume is reduced, but the ability to maintain hermetic sealing at high pressures becomes difficult

Engineering Contradiction:
Improvetank volumeVSAvoidhermetic sealing capability
Core Design Contradiction:
Volume of stationary objectVSReliability

Solution Approach 1:

The patent employs flexible sealing elements and thin-film diaphragms that can maintain hermetic sealing in small-volume tanks under high pressure. These flexible components deform elastically to accommodate pressure variations while maintaining seal integrity, enabling reliable operation in the 3-20 cm3 volume range at pressures up to 400 bar.

Inventive Principle:
Principle #30Flexible shells and thin films

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The device achieves precise separation of gases, hydrocarbons, and water with reduced system dead volumes, enabling efficient operation at high pressures and improving measurement accuracy in micro-scale laboratory settings.

Implementation Method 1

the device is equipped with two RC oscillator circuits that measure the variation in the electric capacity of the electric condensers formed by the measurement probes and the tank walls

Methodology Applied
Scientific EffectCapacitance: Capacitance

Implementation Method 2

the fluids contained in the tank act as a dielectric

Methodology Applied
Scientific EffectDielectric: Dielectric

Implementation Method 3

incorporating a refrigeration system for condensation

Methodology Applied
Scientific EffectCondensation: Condensation

Data Source

PatentUS8800301B2Capacitive separator device
Publication Date: 2014.08.12 CONSEJO SUPERIOR DE INVESTIGACIONES CIENTIFICAS (CSIC)
  • US8800301B2 patent drawing
  • US8800301B2 patent drawing
  • US8800301B2 patent drawing

AI summary

A device is disclosed which is designed to separate water, hydrocarbons and gases, based on the electric characteristics of the materials; the device utilizes the different capacitance of water and hydrocarbons.