Capacitor Film Cast Raw Sheet Beta-Form Control

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Solution Overview

Problem

Current capacitor films face challenges in achieving high voltage resistance, processing suitability, and high electric capacity due to the trade-off between surface roughness and crystallinity, which affects extensibility and film thickness.

Innovation Solution

A cast raw sheet for capacitor films is developed using a polypropylene resin with a weight average molecular weight of 100,000 to 500,000, a molecular weight distribution of 7 or more, and containing 97% isotactic components, with a β-form proportion of 1% to 20%, produced through slurry polymerization and sequential extraction, allowing for balanced stereoregularity and extensibility.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of operation

If the surface is roughened by forming β-form to improve processing suitability, then the processing suitability for winding elements is improved, but the voltage resistance deteriorates

Engineering Contradiction:
Improveprocessing suitabilityVSAvoidvoltage resistance
Core Design Contradiction:
Ease of operationVSReliability

Solution Approach 1:

The patent applies parameter changes by precisely controlling the β-form content within 1-20% range and molecular weight distribution (Mw/Mn) of 7 or more. This optimization allows the surface to have sufficient roughness for processing suitability while limiting excessive roughness that would harm voltage resistance, thereby resolving the contradiction between ease of operation and reliability

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent applies local quality by creating fine unevenness specifically on the film surface through controlled β-form generation, while maintaining the bulk material's high crystallinity and stereoregularity. This localized surface modification improves processing suitability without compromising the overall voltage resistance of the film

Inventive Principle:
Principle #3Local quality

2Reliability

If the crystallinity is increased to improve voltage resistance, then the voltage resistance is improved, but the extensibility deteriorates

Engineering Contradiction:
Improvevoltage resistanceVSAvoidextensibility
Core Design Contradiction:
ReliabilityVSEase of manufacture

Solution Approach 1:

The patent resolves this contradiction by optimizing the molecular weight distribution parameter (Mw/Mn ≥ 7) and controlling β-form content (1-20%). These parameter changes enable the material to achieve both high crystallinity for voltage resistance and sufficient extensibility for manufacturing, as the broad molecular weight distribution provides chain flexibility while high stereoregularity ensures crystallinity

Inventive Principle:
Principle #35Parameter changes

3Quantity of substance

If the film thickness is reduced to improve electric capacity, then the electric capacity is improved, but the mechanical strength deteriorates

Engineering Contradiction:
Improveelectric capacityVSAvoidmechanical strength
Core Design Contradiction:
Quantity of substanceVSStrength

Solution Approach 1:

The patent applies parameter changes by optimizing the molecular weight (100,000-500,000) and molecular weight distribution (Mw/Mn ≥ 7). These parameters enable the production of extremely thin films with maintained mechanical strength, as the broad molecular weight distribution provides chain entanglement and flexibility even at reduced thickness, supporting both high electric capacity and mechanical integrity

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution results in a capacitor film with high voltage resistance, excellent processing suitability, and high electric capacity, enabling the production of extremely thin films suitable for capacitors while maintaining mechanical strength and surface roughness.

Implementation Method 1

When a molten polypropylene resin is crystallized within a particular temperature range, the β-form is generated. When this β-form is drawn at the vicinity of the melting point thereof, a spherulite of β-form transfers to a spherulite of α-form with a density different from that of β-form. The density-difference between these crystal forms generates fine unevenness on the film surface.

Methodology Applied
Scientific EffectCrystallization: Crystallisation

Implementation Method 2

When this β-form is drawn at the vicinity of the melting point thereof, a spherulite of β-form transfers to a spherulite of α-form with a density different from that of β-form.

Methodology Applied
Scientific EffectPhase transition: Phase Change

Data Source

PatentUS9548160B2Raw sheet for capacitor film and capacitor film
Publication Date: 2017.01.17 OJI HLDG CORP

AI summary

A cast raw sheet for a capacitor film, prepared by heating and melting a polypropylene resin and extruding the resin from a T-die, wherein the polypropylene resin has: a weight average molecular weight, determined by gel permeation chromatography, of 100,000 or more and 500,000 or less; and a molecular weight distribution Mw/Mn of 7 or more, the resin contains 97% by mass or more of an isotactic component that is an extraction residue obtained by sequential extraction, and the cast raw sheet contains a β-form in a proportion of 1% or more and less than 20%, the proportion being determined by X-ray diffraction intensity.