Capillary Jet Emulsion Device for Micron Droplets

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Solution Overview

Problem

Current methods for generating micro- and submicrometric emulsions face limitations such as dependency on electrical properties, low productivity, alignment issues with flow-focusing devices, and inability to produce droplets smaller than 5 microns, particularly in the food, pharmaceutical, and chemical industries.

Innovation Solution

A device and process utilizing coaxial flow of immiscible liquids with a viscous outer fluid to form capillary jets, which break up into monodisperse micrometre-sized droplets, eliminating the need for electric fields and addressing geometrical focusing problems, allowing for controlled production of simple and compound emulsions with controllable diameters and coatings.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If electrospraying is used to produce micrometre-sized emulsions, then droplet size control is improved, but productivity deteriorates due to low mass flow rate

Engineering Contradiction:
Improvedroplet size controlVSAvoidmass flow rate
Core Design Contradiction:
Manufacturing precisionVSProductivity

Solution Approach 1:

The invention replaces the electrospraying method (which uses electrical fields) with a purely mechanical flow-focusing system. The capillary tube array focuses the inner liquid stream mechanically through geometric constraints, eliminating the need for electrical fields while maintaining precise droplet size control through the capillary dimensions and flow rates.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

2Manufacturing precision

If flow-focusing devices with three-dimensional geometries are used, then droplet size control is improved, but device complexity increases

Engineering Contradiction:
Improvedroplet size controlVSAvoidgeometrical complexity
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The invention segments the flow-focusing function into multiple independent capillary tubes arranged in an array. Each capillary tube independently focuses a portion of the inner liquid stream, and their combined effect produces the desired droplet size control. This segmentation simplifies the overall device geometry compared to complex three-dimensional focusing structures while maintaining precision.

Inventive Principle:
Principle #1Segmentation

3Manufacturing precision

If electrospraying is used to achieve droplet sizes below 5 microns, then manufacturing precision is improved, but device complexity and operational constraints increase

Engineering Contradiction:
Improvedroplet size controlVSAvoidphysical-chemical parametric freedom
Core Design Contradiction:
Manufacturing precisionVSAdaptability or versatility

Solution Approach 1:

The invention replaces the electrical field-based electrospraying mechanism with a mechanical flow-focusing mechanism using capillary tubes. This substitution eliminates the dependency on electrical properties of the liquid, providing physical-chemical parametric freedom while achieving droplet sizes below 5 microns through purely mechanical means.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

4Manufacturing precision

If flow-focusing devices with alignment requirements are used, then manufacturing precision is improved, but ease of operation deteriorates due to alignment sensitivity

Engineering Contradiction:
Improvedroplet size controlVSAvoidalignment sensitivity
Core Design Contradiction:
Manufacturing precisionVSEase of operation

Solution Approach 1:

The invention segments the focusing function into multiple capillary tubes that can be independently positioned and aligned. This segmentation allows for modular assembly and adjustment, reducing the overall alignment sensitivity compared to single complex focusing structures. Each capillary tube operates independently, so minor misalignments do not compromise the entire system.

Inventive Principle:
Principle #1Segmentation

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Enables the production of stable, uniform, and continuous emulsions with droplet sizes ranging from 10 to 100 microns, addressing the limitations of existing technologies by achieving efficient and scalable generation of micrometre-sized emulsions without the need for electric fields or complex geometries.

Implementation Method 1

a capillary micro-jet when a liquid or two immiscible or barely miscible liquids that flow coaxially are suctioned by means of a viscous outer liquid

Methodology Applied
Scientific EffectCapillary flow: Capillary Action

Implementation Method 2

the action of the co-flowing outer liquid and the favourable pressure gradient that it produces

Methodology Applied
Scientific EffectPressure gradient: Pressure Gradient

Implementation Method 3

This simple jet breaks up due to capillary instability, to produce droplets of a micro- and submicrometric size

Methodology Applied
Scientific EffectCapillary instability: Plateau-Rayleigh Instability

Data Source

PatentEP3187252B1Method and device for producing simple and compound micrometre-sized emulsions
Publication Date: 2020.12.30 DEL CAMPO CORTES FRANCISCO
  • EP3187252B1 patent drawingFigure 1
  • EP3187252B1 patent drawingFigure 2

AI summary

The invention relates to a method for producing simple and compound emulsions having micrometre-sized, controllable diameters and coatings, using a device formed by elements having characteristic dimensions of the order of a millimetre. The emulsions are produced using the suction produced by the flow of a viscous liquid through the section of a millimetre-sized capillary tube. According to a parametric analysis, the liquid or the pair of liquids to be emulsified form a simple or compound steady capillary jet of micrometre diameter, by the action of the co-flow of the emulsifying liquid and the favourable pressure gradient produced. The jet breaks because of capillary instability, forming simple or compound monodisperse micro-drops. The invention disclosed in this description can be used in industrial sectors where the production of simple and compound, monodisperse, homogeneous emulsions having micrometric-sized, controllable diameters and coatings is an essential part of the process.