Capillary Pore Alteration via Sequential Fluid Flow

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Solution Overview

Problem

Current technologies face challenges in controlling the alteration of pores, particularly in creating complex structures within small capillaries and optical fibers, which limits the fabrication of high-density electrical and optical conductors and fibers.

Innovation Solution

The method involves using sequential fluid flow of surface-altering materials to deposit and remove materials within porous substrates through controlled reactions, such as self-assembly, electrochemical deposition, and chemical reactions, allowing for the formation of microscopic structures with high aspect ratios and complex geometries.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If conventional fabrication methods are used to create small electrical conductors and optical fibers, then manufacturing simplicity is maintained, but manufacturing precision and structural complexity are limited

Engineering Contradiction:
Improveprecision of pore alterationVSAvoidcomplexity of fabrication process
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The fabrication process is segmented into distinct sequential steps: pore formation, material deposition, and material removal. Each step is independently controlled through fluid flow, enabling precise manipulation of pore structures without requiring complex integrated processes

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The invention controls pore alteration by changing fluid flow parameters (flow rate, composition, pressure) to precisely control deposition and removal rates. This allows dynamic adjustment of structural complexity and precision during fabrication

Inventive Principle:
Principle #35Parameter changes

2Manufacturing precision

If material is deposited radially inwardly on pore walls to form structures, then manufacturing precision of microscopic structures is improved, but loss of pore volume increases

Engineering Contradiction:
Improveprecision of microscopic structure formationVSAvoidloss of pore volume
Core Design Contradiction:
Manufacturing precisionVSLoss of substance

Solution Approach 1:

The fabrication employs periodic alternation between deposition phases (building structures) and removal phases (clearing excess material). This periodic action enables precise control over final pore volume and structure formation, achieving high precision while minimizing net material loss

Inventive Principle:
Principle #19Periodic action

Solution Approach 2:

Material deposition and removal are localized to specific pore regions through controlled fluid flow patterns. This allows selective alteration of pore walls where needed while preserving overall pore volume and structure in other regions

Inventive Principle:
Principle #3Local quality

3Manufacturing precision

If sequential fluid flow is used to deposit and remove materials in pores, then manufacturing precision of complex geometries is improved, but productivity decreases due to sequential processing

Engineering Contradiction:
Improveprecision of complex geometry fabricationVSAvoidfabrication rate
Core Design Contradiction:
Manufacturing precisionVSProductivity

Solution Approach 1:

Multiple fabrication operations (deposition, removal, cleaning) are merged into a single sequential fluid flow process. By combining these steps into one continuous workflow with automated fluid switching, the invention maintains high precision while improving productivity compared to separate manual processes

Inventive Principle:
Principle #5Merging (Combining)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enables the precise creation of microscopic structures and assemblies with high aspect ratios, facilitating the development of advanced microelectrodes and opto-electrode arrays for enhanced electrochemical and optical analysis, with applications in chemistry, biology, and medicine.

Implementation Method 1

maintaining the stream until a layer is built up along an inner wall of the capillary from material deposited from the flowing stream

Methodology Applied
Scientific EffectDeposition: Deposition (physical)

Implementation Method 2

by selectively depositing materials on the substrate walls using controlled reactions (e.g., by self assembly, electrochemical deposition, electroless deposition, in situ polymerization, biological reaction, and/or chemical reaction, hereinafter termed 'deposition')

Methodology Applied
Scientific EffectChemical reaction: Chemical Bonding

Implementation Method 3

The deposition and removal process is achieved using fluid flow to transport materials into pores and to enable the controlled deposition or removal of materials

Methodology Applied
Scientific EffectFluid flow: Convection

Implementation Method 4

establishing a flowing stream of a solution containing a colloidal suspension of particles within the capillaries and maintaining the flowing stream of the colloidal suspension of particles until a layer of particles is built up on the bonding layer

Methodology Applied
Scientific EffectColloidal suspension: Colloid

Data Source

PatentUS8663973B2Controlled alteration of pores using fluid flow and fabrication of articles thereby
Publication Date: 2014.03.04 TUFTS UNIV
  • US8663973B2 patent drawing
  • US8663973B2 patent drawing
  • US8663973B2 patent drawing

AI summary

The invention relates to microscopic structures and methods of making and using the structures. A method of forming a microscopic structure of a material includes obtaining a solution (310) containing the material, establishing a flowing stream of the solution (310) in a capillary (104), wherein the capillary (104) has an inner dimension that is smaller than about 300 micrometers, and maintaining the stream until a layer is built up along an inner wall of the capillary (104) from material deposited from the flowing stream, thereby forming a microscopic structure.