Carbon Black Dispersion Using Polyamic Acid

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Solution Overview

Problem

Conventional methods for manufacturing carbon black dispersion often result in poor dispersion efficiency and prolonged processing times, leading to carbon black compositions with inadequate thermal resistance due to the use of dispersants with low thermal stability.

Innovation Solution

The use of polyamic acid in a solvent containing N,N,N',N'-tetramethyl urea to disperse carbon black, achieving a high carbon black content of 50 to 99% by mass, which enhances thermal resistance and dispersion efficiency.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If conventional dispersants are used to disperse carbon black in organic solvents, then carbon black can be dispersed, but the dispersion efficiency is poor and processing time is extended

Engineering Contradiction:
Improvedispersion efficiencyVSAvoidprocessing time
Core Design Contradiction:
ProductivityVSLoss of time

Solution Approach 1:

The invention changes the chemical parameters of the dispersant system by using polyamic acid with specific functional groups instead of conventional dispersants. This parameter change enables faster dispersion kinetics and improved dispersion efficiency while reducing processing time

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention creates a composite dispersant system combining polyamic acid with specific functional groups that work synergistically to disperse carbon black. This composite approach achieves both high dispersion efficiency and reduced processing time

Inventive Principle:
Principle #40Composite materials

2Reliability

If conventional dispersants with low thermal stability are used, then carbon black dispersion can be achieved, but the resulting composition has poor thermal resistance

Engineering Contradiction:
Improvethermal resistanceVSAvoiddispersant selection
Core Design Contradiction:
ReliabilityVSEase of manufacture

Solution Approach 1:

The invention changes the thermal stability parameter of the dispersant by selecting polyamic acid which inherently possesses high thermal resistance. This parameter change ensures the final composition maintains excellent thermal resistance while remaining easy to manufacture

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention replaces conventional dispersants that require careful thermal management with polyamic acid that inherently withstands high temperatures, simplifying the manufacturing process and improving product reliability

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

3Quantity of substance

If carbon black content is increased to achieve desired black density, then coloring performance improves, but dispersion difficulty increases

Engineering Contradiction:
Improvecarbon black contentVSAvoiddispersion difficulty
Core Design Contradiction:
Quantity of substanceVSDevice complexity

Solution Approach 1:

The invention changes the interfacial parameters between carbon black and dispersant by using polyamic acid with specific functional groups. This parameter change allows high carbon black content (50-99% by mass) to be achieved while maintaining easy dispersion and avoiding aggregation

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This method provides a carbon black dispersion with improved thermal resistance and faster dispersion times, resulting in a black composition with desired density and stability, suitable for various applications including ink and resin compositions.

Implementation Method 1

dispersing carbon black by using polyamic acid in a solvent containing N,N,N’,N’-tetramethyl urea

Methodology Applied
Scientific EffectDispersion: Dispersion (of waves)

Data Source

PatentEP2910611B1Carbon black dispersion
Publication Date: 2016.12.07 TOKYO OHKA KOGYO CO LTD
  • EP2910611B1 patent drawing
  • EP2910611B1 patent drawing
  • EP2910611B1 patent drawing

AI summary

The problem to be solved by the present invention is: to provide a carbon black dispersion containing well-dispersed carbon black and giving a black composition superior in thermal resistance; to provide a black composition giving a black shaped body which is colored in black of a desired density and superior in thermal resistance; and to provide a dispersion method of carbon black that allows preferable dispersion of carbon black in a short period of time, and preparation of a carbon black dispersion that gives a black composition superior in thermal resistance. In order to solve the above described problems, carbon black is dispersed in a solvent containing N,N,N',N'-tetramethyl urea, by using polyamic acid.