Carbon/Carbon Composite Impregnation for Uniform Ceramic Distribution

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Solution Overview

Problem

Existing carbon/carbon composite materials exhibit non-homogeneous distribution of ceramic particles, leading to heterogeneity in mechanical properties and reduced service life, making renovation difficult.

Innovation Solution

A manufacturing method involving controlled viscosity of the impregnation solution to ensure homogeneous distribution of ceramic fillers, using sol-gel or colloidal dispersion with additives to maintain viscosity between 12 and 700 mPa s, followed by drying and heat treatment to achieve uniform ceramic particle distribution.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Strength

If ceramic particles are introduced to improve mechanical properties, then wear resistance is improved, but distribution homogeneity deteriorates

Engineering Contradiction:
Improvewear resistanceVSAvoiddistribution homogeneity
Core Design Contradiction:
StrengthVSStability of the object's composition

Solution Approach 1:

The patent changes the physical-chemical parameters of the impregnation solution, specifically controlling viscosity within the range of 12-700 mPa·s and adjusting ceramic particle concentration (3-15% by mass). These parameter changes ensure optimal flow characteristics during impregnation while maintaining homogeneous distribution of ceramic particles throughout the carbon preform, resolving the contradiction between wear resistance improvement and distribution homogeneity.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent ensures that the impregnation solution penetrates uniformly throughout the entire volume of the carbon preform, achieving consistent ceramic particle distribution in all regions (core and periphery). This local quality control through optimized viscosity and concentration ensures homogeneous reinforcement throughout the material, preventing the heterogeneity that would otherwise occur during drying.

Inventive Principle:
Principle #3Local quality

2Ease of manufacture

If ceramic particles are concentrated at edges during drying, then manufacturing simplicity is maintained, but material heterogeneity increases

Engineering Contradiction:
Improvemanufacturing simplicityVSAvoidmaterial homogeneity
Core Design Contradiction:
Ease of manufactureVSStability of the object's composition

Solution Approach 1:

The patent applies preliminary action by optimizing the viscosity of the impregnation solution before the drying process begins. By controlling viscosity to 12-700 mPa·s and adjusting ceramic concentration to 3-15% by mass, the solution achieves proper penetration and distribution of ceramic particles throughout the preform before drying occurs. This preliminary optimization prevents the harmful concentration gradient that would otherwise form during drying, maintaining homogeneity without complicating the manufacturing process.

Inventive Principle:
Principle #10Preliminary action

3Device complexity

If impregnation solution viscosity is not controlled, then process complexity is reduced, but particle distribution homogeneity deteriorates

Engineering Contradiction:
Improveprocess complexityVSAvoidparticle distribution homogeneity
Core Design Contradiction:
Device complexityVSStability of the object's composition

Solution Approach 1:

The patent introduces control of the viscosity parameter of the impregnation solution, maintaining it within 12-700 mPa·s, and adjusts ceramic particle concentration to 3-15% by mass. These parameter changes are implemented through straightforward formulation adjustments rather than complex process equipment, achieving homogeneous particle distribution while keeping the manufacturing process relatively simple and industrially viable.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Results in a carbon/carbon composite material with homogeneous properties throughout its life, enabling effective renovation and extended service life.

Implementation Method 1

the impregnation of the partially densified blank with an impregnation solution including ceramic precursors or ceramic particles

Methodology Applied
Scientific EffectCapillary action: Capillary Action

Implementation Method 2

the drying of the impregnated blank

Methodology Applied
Scientific EffectEvaporation: Evaporation

Data Source

PatentUS12577173B2Method for manufacturing a part made of carbon/carbon composite material with improved mechanical properties
Publication Date: 2026.03.17 SAFRAN LANDING SYSTEMS
  • US12577173B2 patent drawing
  • US12577173B2 patent drawing

AI summary

Method for manufacturing a part made from carbon/carbon composite material, comprising:the formation of a carbonaceous preform,partial densification of the preform by a pyrocarbon matrix thus forming a partially densified blank,the impregnation of the partially densified blank with an impregnation solution including ceramic particles or ceramic precursors, andthe drying of the impregnated blank.Furthermore, the viscosity of the dispersion or impregnation solution is controlled in order to control the homogeneity of the distribution of the ceramic particles in the part of the impregnated composite material during drying.