Carbonaceous Composition Processing System for High-Rate Graphite Oxide Synthesis

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Solution Overview

Problem

Current methods for processing carbonaceous compositions, such as graphite oxide and reduced graphite oxide, face challenges in efficiently manufacturing and processing these materials at large scales while maintaining quality and productivity.

Innovation Solution

A system comprising a reaction vessel and a tank with agitators and sensors, which allows for the controlled agitation and temperature regulation of carbonaceous compositions, enabling the production of oxidized and reduced forms of carbonaceous materials at high rates, including the synthesis of graphite oxide and reduced graphite oxide.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If conventional methods are used for processing carbonaceous compositions, then manufacturing simplicity is maintained, but productivity is limited and cannot achieve rates greater than 1 tonne per year

Engineering Contradiction:
Improvemanufacturing rateVSAvoidsystem complexity
Core Design Contradiction:
ProductivityVSDevice complexity

Solution Approach 1:

The manufacturing system is divided into separate functional modules: a reaction vessel for oxidation, a tank for reduction, and associated agitation systems. This segmentation allows each component to be optimized independently while working together to achieve high-volume production of oxidized and reduced carbonaceous compositions at rates exceeding 1 tonne per year

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The system integrates multiple functions into a unified manufacturing platform that can produce both oxidized forms (graphite oxide) and reduced forms (reduced graphite oxide) of carbonaceous compositions. The reaction vessel and tank can handle different chemical processes sequentially or simultaneously, enabling versatile production of various carbon-based materials for capacitor applications

Inventive Principle:
Principle #6Universality (Multi-functionality)

2Productivity

If large-scale processing is implemented, then productivity increases, but maintaining quality and consistency becomes more difficult

Engineering Contradiction:
Improvemanufacturing rateVSAvoidmaterial quality
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

The system incorporates agitation control mechanisms that maintain consistent mixing conditions throughout the reaction and reduction processes. By ensuring uniform distribution of reactants and consistent shear conditions, the system produces homogeneous products with repeatable properties across large production volumes, maintaining material quality while achieving high productivity

Inventive Principle:
Principle #23Feedback

Solution Approach 2:

The manufacturing process utilizes controlled changes in chemical parameters (oxidation state, reduction level) and physical parameters (agitation rate, temperature) to optimize both production volume and material quality. By systematically adjusting these parameters, the system can produce consistent high-quality carbonaceous compositions suitable for capacitor electrodes at scaled production rates

Inventive Principle:
Principle #35Parameter changes

3Productivity

If high-rate production is achieved, then productivity exceeds 1 tonne per year, but process control and temperature regulation become more challenging

Engineering Contradiction:
Improvemanufacturing rateVSAvoidtemperature control
Core Design Contradiction:
ProductivityVSTemperature

Solution Approach 1:

The system performs oxidation in the reaction vessel before transferring to the tank for reduction, allowing temperature and reaction conditions to be optimized separately for each stage. This preliminary action enables better thermal management at high production rates by preventing heat accumulation and maintaining controlled temperatures throughout the multi-step process

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The system effectively processes carbonaceous compositions to produce high-quality oxidized and reduced forms at rates greater than 1 tonne per year, suitable for applications in capacitors with peak capacitance of at least 100 mF/cm², enhancing productivity and material quality.

Implementation Method 1

forming an oxidized form of the carbonaceous composition

Methodology Applied
Scientific EffectOxidation: Oxidation

Data Source

PatentUS11752479B2Methods, devices and systems for processing of carbonaceous compositions
Publication Date: 2023.09.12 NANOTECH ENERGY INC
  • US11752479B2 patent drawing
  • US11752479B2 patent drawing
  • US11752479B2 patent drawing

AI summary

Provided herein are methods, devices and systems for processing of carbonaceous compositions. The processing may include the manufacture (or synthesis) of oxidized forms of carbonaceous compositions and/or the manufacture (or synthesis) of reduced forms of oxidized carbonaceous compositions. Some embodiments provide methods, devices and systems for the manufacture (or synthesis) of graphite oxide from graphite and/or for the manufacture (or synthesis) of reduced graphite oxide from graphite oxide.