Carboxylic Acid Dry Development of Metal-Containing Resist Films

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Solution Overview

Problem

Existing technologies face challenges in appropriately dry-developing exposed metal-containing resist films, which is crucial for precise substrate processing in semiconductor manufacturing.

Innovation Solution

A method for processing a substrate involves providing a substrate with a metal-containing resist film having distinct regions, and then dry-developing the resist film by exposing it to a processing gas containing carboxylic acid, with a pressure or partial pressure of the carboxylic acid maintained between 0.3 Torr and 100 Torr.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If conventional dry development is used on metal-containing resist, then the process is simple, but the development precision and selectivity are insufficient

Engineering Contradiction:
Improvedevelopment precisionVSAvoidprocess complexity
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The patent applies parameter changes by optimizing the pressure or partial pressure of carboxylic acid to be 0.3 Torr or more and less than 100 Torr. This specific parameter range enables appropriate dry development of metal-containing resist by controlling the reaction conditions, thereby achieving high development precision while maintaining process feasibility

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent employs local quality by using carboxylic acid that selectively reacts with exposed metal-containing resist regions. The processing gas contains carboxylic acid at controlled concentration, which selectively removes the second region (exposed area) while preserving the first region (unexposed area), achieving high selectivity in development

Inventive Principle:
Principle #3Local quality

2Productivity

If high pressure of carboxylic acid is used, then development speed increases, but selectivity and control precision decrease

Engineering Contradiction:
Improvedevelopment speedVSAvoidselectivity
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

The patent resolves this contradiction by defining a specific pressure range for carboxylic acid (0.3 Torr or more and less than 100 Torr). This optimized parameter range balances development speed and selectivity, preventing both too-slow development (at very low pressure) and loss of selectivity (at very high pressure)

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This method enables appropriate dry-development of the metal-containing resist, ensuring selective removal of specific regions with high precision and control, thereby improving the substrate processing outcomes.

Implementation Method 1

dry-developing the resist film by supplying a processing gas containing a carboxylic acid into the processing chamber, exposing the substrate to the carboxylic acid, and selectively removing the second region with respect to the first region

Methodology Applied
Scientific EffectChemical reaction: Chemical Bonding

Data Source

PatentEP4557004A1Method for processing substrate, and system for processing substrate
Publication Date: 2025.05.21 TOKYO ELECTRON LTD
  • EP4557004A1 patent drawingFigure 1
  • EP4557004A1 patent drawingFigure 2
  • EP4557004A1 patent drawingFigure 3

AI summary

A method for processing a substrate is provided. The method for processing a substrate includes (a) providing a substrate on a substrate support in a processing chamber, the substrate having an underlying film and a resist film disposed on the underlying film and formed of a metal-containing resist, and the resist film having a first region and a second region. The method for processing a substrate further includes (b) dry-developing the resist film by supplying a processing gas containing a carboxylic acid into the processing chamber, exposing the substrate to the carboxylic acid, and selectively removing the second region with respect to the first region. In the (b), a pressure or a partial pressure of the carboxylic acid is 0.3 Torr (40 Pa) or more and less than 100 Torr (13,332 Pa).