Catalyst Production Apparatus Washing with Basic Solution

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Solution Overview

Problem

Conventional methods for producing catalysts containing molybdenum, bismuth, and iron result in unstable physical properties and reduced catalyst activity and selectivity due to adherence of solid matter on production apparatus surfaces, affecting reproducibility.

Innovation Solution

A method involving the washing of apparatus surfaces with a basic solution to remove residual materials containing molybdenum, bismuth, and iron, thereby stabilizing the physical properties and maintaining catalyst activity and selectivity.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If catalyst production is repeated without washing the apparatus, then production efficiency is maintained, but physical properties of dried material and catalyst activity deteriorate due to solid matter accumulation

Engineering Contradiction:
Improveproduction efficiencyVSAvoidcatalyst activity and selectivity
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The apparatus surface is washed with a basic solution before the next catalyst production batch to remove accumulated solid matter. This preliminary cleaning action prevents the deterioration of catalyst properties in subsequent productions, resolving the contradiction between maintaining production efficiency and ensuring catalyst reliability.

Inventive Principle:
Principle #10Preliminary action

2Manufacturing precision

If apparatus is washed frequently to maintain catalyst quality, then catalyst reproducibility improves, but production time and operational complexity increase

Engineering Contradiction:
Improvecatalyst reproducibilityVSAvoidwashing time
Core Design Contradiction:
Manufacturing precisionVSLoss of time

Solution Approach 1:

A basic solution is used for washing instead of water or other solutions, as the basic conditions specifically effectively remove the solid matter containing molybdenum, bismuth, and iron. This parameter change (using basic solution) enables effective cleaning with minimal washing time, improving catalyst reproducibility without excessive time loss.

Inventive Principle:
Principle #35Parameter changes

3Quantity of substance

If solid matter adheres to apparatus surface, then residual material remains in system, but this causes change in bulk density and deterioration of catalyst properties

Engineering Contradiction:
Improveresidual materialVSAvoidbulk density stability
Core Design Contradiction:
Quantity of substanceVSStability of the object's composition

Solution Approach 1:

The basic solution washing process extracts and removes the solid matter containing molybdenum, bismuth, and iron from the apparatus surface. By taking out this residual material, the bulk density stability and catalyst composition consistency are maintained across production batches.

Inventive Principle:
Principle #2Taking out (Extraction)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method ensures stable physical properties and improved reproducibility of catalysts, reducing the need for frequent apparatus overhauls and enhancing catalyst performance.

Implementation Method 1

washing a surface of at least one device equipped in an apparatus for the production of catalyst, to which a solid matter adheres, with a basic solution

Methodology Applied
Scientific EffectChemical dissolution:

Data Source

PatentUS8563774B2Method for producing catalyst
Publication Date: 2013.10.22 MITSUBISHI CHEM CORP

AI summary

Disclosed is a method for producing a catalyst, in which physical properties of a dried material or a calcined material in a production process of the catalyst are stable and a change in at least one of a catalyst activity and a selectivity to a target product is small and hence reproducibility of the catalyst is excellent. The present invention is a method for producing a catalyst containing molybdenum, bismuth, and iron, which contains the steps of washing a surface of at least one device equipped in an apparatus for the production of catalyst, to which a solid matter adheres, with a basic solution, and producing the catalyst with the apparatus for the production of catalyst thus washed.