Composite Cathode Coating for Nickel-Rich Cycle and Thermal Stability

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Solution Overview

Problem

Nickel-based cathode active materials in lithium batteries suffer from degraded lifespan characteristics and poor thermal stability due to side reactions, necessitating a solution to prevent or reduce battery performance deterioration.

Innovation Solution

A composite cathode active material is developed, comprising a core of lithium transition metal oxide coated with a shell containing lithium nitrate, conductive carbon-based composite, and first metal oxides, such as Al, Nb, Mg, Sc, Ti, Zr, V, W, Mn, Fe, Co, Pd, Cu, Ag, Zn, and Se, embedded in a graphene matrix, which enhances ion conduction and prevents side reactions.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Use of energy by moving object

If nickel-based cathode active materials are used to achieve high capacity, then energy density is improved, but lifespan characteristics and thermal stability deteriorate due to side reactions

Engineering Contradiction:
Improveenergy densityVSAvoidlifespan characteristics
Core Design Contradiction:
Use of energy by moving objectVSReliability

Solution Approach 1:

The patent applies composite materials by creating a core-shell structure where the core is lithium transition metal oxide (providing high capacity) and the shell contains lithium nitrate, conductive carbon-based composite, and first metal oxides embedded in graphene matrix. This composite structure allows the high-capacity nickel-based core to be protected by the stable shell, resolving the contradiction between achieving high energy density and maintaining reliability.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The patent uses a thin shell layer conforming to the core surface that acts as a protective barrier. This shell prevents direct contact between the nickel-based core and electrolyte, reducing side reactions while maintaining the high capacity benefits of the nickel-based material, thus improving lifespan characteristics without sacrificing energy density.

Inventive Principle:
Principle #30Flexible shells and thin films

2Use of energy by moving object

If nickel-based cathode active materials are used to achieve high capacity, then energy density is improved, but thermal stability deteriorates due to side reactions

Engineering Contradiction:
Improveenergy densityVSAvoidthermal stability
Core Design Contradiction:
Use of energy by moving objectVSTemperature

Solution Approach 1:

The composite structure combines nickel-based lithium transition metal oxide core with a shell containing lithium nitrate, conductive carbon-based composite, and first metal oxides in graphene matrix. This composite design provides thermal stability through the stable shell components while preserving the high energy density of the nickel-based core.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The thin shell layer acts as a thermal barrier and protective interface, preventing direct thermal and chemical interactions between the nickel-based core and electrolyte. This improves thermal stability while allowing the high-capacity core to function, resolving the contradiction between energy density and thermal stability.

Inventive Principle:
Principle #30Flexible shells and thin films

3Reliability

If a shell is added to prevent side reactions, then reliability is improved, but device complexity increases

Engineering Contradiction:
Improvelifespan characteristicsVSAvoidstructure complexity
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent creates a composite cathode active material where the shell is not a separate component but is integrated with the core to form a unified composite structure. This approach improves reliability by preventing side reactions while avoiding the complexity of assembling separate shell and core components, as the composite is prepared as a single integrated material.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The patent merges the shell and core into a single composite cathode active material structure. The shell components (lithium nitrate, conductive carbon-based composite, first metal oxides in graphene matrix) are combined with the lithium transition metal oxide core to form an integrated composite, simplifying the overall device structure while maintaining the protective function.

Inventive Principle:
Principle #5Merging (Combining)

4Adaptability or versatility

If multiple components are combined in the shell, then functionality is improved, but manufacturing precision requirements increase

Engineering Contradiction:
ImprovefunctionalityVSAvoidcoating uniformity
Core Design Contradiction:
Adaptability or versatilityVSManufacturing precision

Solution Approach 1:

The patent prepares the composite cathode active material as a single integrated composite through mechanical mixing and milling of all components (lithium transition metal oxide, lithium nitrate, conductive carbon-based composite, and first metal oxides in graphene matrix). This approach allows multiple functional components to be combined in the shell while avoiding the need for precise sequential coating operations, thus maintaining functionality without excessively increasing manufacturing precision requirements.

Inventive Principle:
Principle #40Composite materials

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The composite cathode active material improves the reversibility of electrode reactions, maintains high rate and cycle characteristics, and reduces internal resistance, leading to enhanced lithium battery performance.

Implementation Method 1

the shell includes lithium nitrate, LiNO3; and a conductive carbon-based composite

Methodology Applied
Scientific EffectIon conduction: Conduction (electrical)

Implementation Method 2

a shell conformed to a surface of the core... capable of inhibiting a side reaction of the composite cathode active material

Methodology Applied
Scientific EffectPhysical containment: Physical Containment

Implementation Method 3

mechanically milling the lithium transition metal oxide, the composite, and lithium nitrate

Methodology Applied
Scientific EffectMechanical force: Mechanical Force

Data Source

PatentEP4435901B1Composite cathode active material, cathode and lithium battery including the composite cathode active material, and method of preparing the composite cathode active material
Publication Date: 2025.11.05 SAMSUNG SDI CO LTD
  • EP4435901B1 patent drawingFigure 1
  • EP4435901B1 patent drawingFigure 2
  • EP4435901B1 patent drawingFigure 3

AI summary

A composite cathode active material, a cathode and a lithium battery that include the composite cathode active material, and a method of preparing the composite cathode active material are provided. The composite cathode active material includes: a core including a lithium transition metal oxide; and a shell conformed to a surface of the core, where the shell includes: lithium nitrate and a conductive carbon-based composite, the conductive carbon-based composite includes a first metal oxide represented by MaOb (where 0<a≤3, 0<b<4, and if a is 1, 2, or 3, and b is not an integer); and a carbon-based material; the first metal oxide is in a matrix of the carbon-based material, and M is at least one metal selected from among Groups 2 to 13, 15, and 16 of the Periodic Table of Elements.