CdTe Substrate Surface Treatment for Epitaxial Growth

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Solution Overview

Problem

CdTe-based semiconductor substrates experience surface oxidation and linear polishing damage during storage, leading to decreased epitaxial crystal quality due to uneven oxidation and residual polishing tracks, which are difficult to remove with existing etching methods.

Innovation Solution

A CdTe-based semiconductor substrate with predetermined polishing, etching, and storage treatments to prevent orange peel defects and linear polishing damage, including a light etching treatment of 0.1 µm to 1 µm and storage in a nitrogen gas atmosphere, ensuring no tracks of linear polishing damage are observed by AFM and no orange peel defects are visible under a fluorescent lamp.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If conventional etching treatment is performed to remove oxidation film and polishing damage, then surface oxidation and polishing damage are removed, but linear polishing damage tracks remain and orange peel defects occur

Engineering Contradiction:
Improvesurface qualityVSAvoidlinear polishing damage tracks
Core Design Contradiction:
Manufacturing precisionVSObject-generated harmful factors

Solution Approach 1:

The patent applies preliminary action by performing a controlled etching treatment before substrate storage to remove polishing damage tracks and prevent their propagation. The etching conditions are specifically optimized to eliminate linear polishing damage while maintaining surface planarity, and the substrate is then stored in a nitrogen atmosphere to prevent oxidation during storage and transport, eliminating the need for post-storage etching.

Inventive Principle:
Principle #10Preliminary action

2Object-generated harmful factors

If deep etching is performed to remove all polishing damage, then polishing tracks are removed, but substrate planarity deteriorates and orange peel defects occur

Engineering Contradiction:
Improvepolishing damage tracksVSAvoidsubstrate planarity
Core Design Contradiction:
Object-generated harmful factorsVSShape

Solution Approach 1:

The patent applies parameter changes by precisely controlling etching parameters (etching depth, etching solution concentration, etching time, temperature) to achieve optimal removal of polishing damage tracks while maintaining substrate planarity. The etching depth is controlled within a specific range (0.1-1.0 μm) to remove tracks without creating orange peel defects, and etching conditions are adjusted based on polishing conditions to achieve the best balance between track removal and planarity maintenance.

Inventive Principle:
Principle #35Parameter changes

3Ease of manufacture

If substrate is stored in air atmosphere, then storage is simple, but surface oxidation progresses unevenly and increases polishing damage

Engineering Contradiction:
Improvestorage simplicityVSAvoidsurface oxidation uniformity
Core Design Contradiction:
Ease of manufactureVSManufacturing precision

Solution Approach 1:

The patent applies inert atmosphere by storing the substrate in a nitrogen gas atmosphere after controlled etching treatment. The nitrogen atmosphere prevents oxidation during storage and transport, maintaining the improved surface quality achieved by etching. The substrate container is designed to maintain nitrogen atmosphere, and oxidation is prevented by controlling nitrogen purity and maintaining appropriate storage conditions, eliminating uneven oxidation while keeping storage practical.

Inventive Principle:
Principle #39Inert atmosphere (Inert environment)

4Shape

If no etching treatment is performed, then substrate planarity is maintained, but linear polishing damage tracks remain and decrease epitaxial crystal quality

Engineering Contradiction:
Improvesubstrate planarityVSAvoidepitaxial crystal quality
Core Design Contradiction:
ShapeVSManufacturing precision

Solution Approach 1:

The patent applies partial action by performing a controlled etching treatment that removes only the necessary portion of polishing damage tracks (0.1-1.0 μm depth) without excessive etching that would cause orange peel defects. This partial etching is sufficient to remove tracks that would degrade epitaxial crystal quality while maintaining substrate planarity, achieving the optimal balance between track removal and planarity preservation.

Inventive Principle:
Principle #16Partial or excessive action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Enables the growth of high-quality epitaxial crystals without pre-etching treatment, enhancing the quality and yield of semiconductor devices by maintaining substrate planarity and reducing thickness variation.

Implementation Method 1

storage in a nitrogen gas atmosphere

Methodology Applied
Scientific EffectOxidation prevention: Oxidation

Implementation Method 2

a light etching treatment with a light etching amount of 0.1 µm to 1 µm

Methodology Applied
Scientific EffectEtching:

Data Source

PatentEP2369041B1Cdte semiconductor substrate for epitaxial growth and substrate container
Publication Date: 2014.12.03 JX NIPPON MINING & METALS CORP
  • EP2369041B1 patent drawingFigure 1
  • EP2369041B1 patent drawingFigure 2

AI summary

Provided is a CdTe-based semiconductor substrate for epitaxial growth, which is capable of growing good-quality epitaxial crystals without urging a substrate user to implement etching treatment before the epitaxial growth. A CdTe-based semiconductor substrate, in which tracks of linear polishing damage with a depth of 1 nm or more are not observed within a viewing range of 10 µm × 10 µm when a surface of the substrate is observed by an atomic force microscope, and orange peel defects are not observed when the surface of the substrate is visually observed under a fluorescent lamp, can grow the good-quality epitaxial crystals.