Ce-based Phosphor Composition for High-Efficiency Red Emission

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

Current red phosphors with Eu as the emission center suffer from decreased quantum efficiency under high-output excitation due to long emission lifetimes, leading to brightness saturation, whereas phosphors with Ce as the emission center are more efficient but limited in their application.

Innovation Solution

A phosphor with a crystal phase having a chemical composition Ce x M 3-x-y β 6 γ 11-z, where M is a rare-earth element, β includes Si and Al/Ga, y consists of N and O, and z is optimized to achieve a maximum emission peak in the 600-800 nm range and excitation peak in the 500-600 nm range, enhancing quantum efficiency and stability.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Illumination intensity

If Eu is used as the emission center in red phosphors, then color rendering properties are improved, but quantum efficiency decreases under high-output excitation due to long emission lifetimes causing brightness saturation

Engineering Contradiction:
Improvecolor rendering propertiesVSAvoidquantum efficiency
Core Design Contradiction:
Illumination intensityVSLoss of energy

Solution Approach 1:

The patent changes the emission center element from Eu to Ce, fundamentally altering the emission mechanism. Ce-based phosphors exhibit shorter emission lifetimes and higher quantum efficiency under high-output excitation while maintaining desirable red emission characteristics through controlled composition and crystal structure

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates a composite phosphor system with formula Ce x M 3-x-y β 6 γ 11-z, combining Ce as the primary emission center with rare-earth elements M and controlled substitutions in the β 6 γ 11 matrix. This composite approach optimizes both quantum efficiency and color rendering by leveraging Ce's efficient emission and the host lattice's structural stability

Inventive Principle:
Principle #40Composite materials

2Loss of energy

If Ce is used as the emission center in phosphors, then quantum efficiency is improved, but emission wavelength control in the red region (600-800 nm) is limited

Engineering Contradiction:
Improvequantum efficiencyVSAvoidemission wavelength control
Core Design Contradiction:
Loss of energyVSIllumination intensity

Solution Approach 1:

The patent systematically varies compositional parameters (x, y, z values and element selections) to tune the Ce emission characteristics. By controlling the substitution levels and host lattice composition, the emission wavelength is precisely controlled within the 600-800 nm red region while preserving Ce's high quantum efficiency

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent introduces local structural modifications through element substitutions in the β 6 γ 11 matrix surrounding the Ce emission centers. These local changes in the crystal environment affect the Ce 5d-4f transition energy levels, enabling precise control of emission wavelength without compromising the overall quantum efficiency

Inventive Principle:
Principle #3Local quality

3Illumination intensity

If high-output excitation is applied to Eu-based phosphors, then brightness is improved, but brightness saturation occurs due to long emission lifetimes

Engineering Contradiction:
ImprovebrightnessVSAvoidbrightness stability
Core Design Contradiction:
Illumination intensityVSReliability

Solution Approach 1:

The patent changes the emission center from Eu to Ce, fundamentally altering the emission lifetime characteristic. Ce-based phosphors exhibit shorter emission lifetimes that prevent accumulation of excited states under high-output excitation, thereby eliminating brightness saturation while maintaining high brightness output and improving reliability

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The phosphor exhibits high quantum efficiency even under high-output excitation, preventing brightness saturation and improving color rendering properties and color reproducibility in light-emitting applications.

Implementation Method 1

A phosphor with a crystal phase having a chemical composition Ce x M 3-x-y β 6 γ 11-z... excitation peak in the 500-600 nm range, enhancing quantum efficiency... The phosphor exhibits high quantum efficiency even under high-output excitation

Methodology Applied
Scientific EffectPhotoluminescence: Photoluminescence

Data Source

PatentEP3480280B1Fluorophore and light-emitting device
Publication Date: 2022.09.07 PANASONIC INTELLECTUAL PROPERTY MANAGEMENT CO LTD
  • EP3480280B1 patent drawingFigure 1~2
  • EP3480280B1 patent drawingFigure 3~4
  • EP3480280B1 patent drawingFigure 5~6

AI summary

A phosphor contains a crystal phase having a chemical composition CexM3-x-yβ6γ11-z. M is one or more elements selected from the group consisting of Sc, Y, La, Pr, Nd, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm, Yb, and Lu. β contains Si in an amount of 50 mol% or more of a total mol of β. γ contains N in an amount of 80 mol% or more N of a total mol of γ. x satisfies 0 < x ≤ 0.6. y satisfies 0 ≤ y ≤ 1.0. z satisfies 0 ≤ z ≤ 1.0. The phosphor has a maximum peak of an emission spectrum in a wavelength range of 600 nm or more and 800 nm or less and a first peak of an excitation spectrum in a wavelength range of 500 nm or more and 600 nm or less.