Small-Particle Cellulose Processing for Stable Suspensions

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Solution Overview

Problem

Existing methods for converting lignocellulosic biomass into cellulose are capital intensive, time-consuming, and require harsh toxic chemicals, lacking environmentally friendly and efficient processes for producing small particle size cellulose particles with specific properties.

Innovation Solution

The production of small particle size cellulose particles with a d75 of less than about 8 microns, d50 of 0.4 to 5 microns, aspect ratio of 1 to 1.5, and non-spherical shape is achieved through sub-critical, near-critical, or supercritical fluid treatment of cellulosic substrates, followed by organic solvent processing to form compositions with increased viscosity and suspension stability.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of manufacture

If conventional methods are used to convert lignocellulosic biomass into cellulose, then cellulose can be produced, but the process is capital intensive, time-consuming, and requires harsh toxic chemicals

Engineering Contradiction:
Improvemanufacturing process simplicityVSAvoiduse of harsh toxic chemicals
Core Design Contradiction:
Ease of manufactureVSObject-affected harmful factors

Solution Approach 1:

The patent changes the physical-chemical parameters of the processing fluid from conventional harsh chemicals to sub-critical, near-critical, or supercritical water, which enables cellulose production without toxic chemicals while maintaining effective biomass conversion

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent replaces complex mechanical processing systems with a fluid-based chemical processing system using sub-critical, near-critical, or supercritical water, simplifying the manufacturing process while eliminating the need for harsh toxic chemicals

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

2Reliability

If cellulose particles are produced with small particle size (d75 < 8 microns), then suspension stability and viscosity enhancement are improved, but the manufacturing precision and control difficulty increase

Engineering Contradiction:
Improvesuspension stabilityVSAvoidparticle size control
Core Design Contradiction:
ReliabilityVSManufacturing precision

Solution Approach 1:

The patent controls particle size by adjusting processing parameters such as fluid temperature, pressure, and residence time in the sub-critical, near-critical, or supercritical water treatment, achieving consistent small particle sizes (d75 < 8 microns) with good suspension stability

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent implements particle size monitoring and process adjustment mechanisms to maintain consistent particle size distribution, ensuring both small particle dimensions and high suspension stability through continuous process optimization

Inventive Principle:
Principle #23Feedback

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method produces cellulose particles that significantly enhance viscosity and suspension stability, enabling their use in various applications such as thickened compositions, emulsions, suspensions, food products, and subterranean treatments, while being environmentally friendly.

Implementation Method 1

The production of small particle size cellulose particles with a d75 of less than about 8 microns, d50 of 0.4 to 5 microns, aspect ratio of 1 to 1.5, and non-spherical shape is achieved through sub-critical, near-critical, or supercritical fluid treatment of cellulosic substrates

Methodology Applied
Scientific EffectSupercritical fluid treatment: Supercritical Fluid

Data Source

PatentEP3648742B1Manufacture, isolation, purification, and uses of small particle size cellulose particles and compositions
Publication Date: 2025.12.31 RENMATIX INC
  • EP3648742B1 patent drawingFigure 1
  • EP3648742B1 patent drawingFigure 2
  • EP3648742B1 patent drawingFigure 3

AI summary

This invention relates to compositions comprising cellulose particles and methods for making and using same. This invention also relates to compositions comprising a fluid and particles comprising cellulose. Thus, disclosed herein are methods of manufacture, isolation, purification, and handling of cellulose particles. Also disclosed are uses for cellulose particles as additives in leavened or leavenable food products, or in an emulsion or emulsifiable product, or as a suspension aid, or in a thickened composition, or in a meat or meat analog product, or in a personal care formulation, or in a beauty formulation, or in a cosmetic formulation, or in a skin care formulation. Also disclosed are uses for cellulose particles in subterranean treatment compositions. Also disclosed are uses for cellulose particles in metal working compositions, cutting compositions, and stamping compositions. Also disclosed herein are resuspendable particles comprising cellulose. This abstract is intended as a scanning tool for purposes of searching in the particular art and is not intended to be limiting of the present invention.