Cellulose Nanofiber Powder Sizing to Prevent Drying Agglomeration

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Solution Overview

Problem

Dried cellulose nanofibers tend to aggregate and solidify, rapidly absorb water, and are difficult to handle and transport due to high hydrophilicity, leading to increased costs and inefficiencies.

Innovation Solution

Forming a powder with specific particle size, water content, and structural properties such as angle of repose and fall, pH, to prevent aggregation and improve handling and transfer efficiency.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If cellulose nanofibers are dried to form a dried product, then packaging and storage costs are reduced, but the dried product aggregates and solidifies, forming lumps that are difficult to handle

Engineering Contradiction:
Improvewater contentVSAvoidhandling ease
Core Design Contradiction:
Quantity of substanceVSEase of operation

Solution Approach 1:

The patent applies parameter changes by controlling the particle size distribution (D10 ≤ 10 μm, D50 ≤ 45 μm) and water content (≤ 20% by mass) of the dried cellulose nanofiber powder. These parameter optimizations prevent aggregation and solidification during drying and storage, while maintaining ease of handling and transfer efficiency.

Inventive Principle:
Principle #35Parameter changes

2Quantity of substance

If cellulose nanofibers are dried to form a dried product, then storage and transportation costs are reduced, but the dried product has high hydrophilicity and rapidly absorbs water, adhering to various places

Engineering Contradiction:
Improvewater contentVSAvoidwater absorption
Core Design Contradiction:
Quantity of substanceVSObject-affected harmful factors

Solution Approach 1:

The patent optimizes the water content parameter to ≤ 20% by mass and controls particle size distribution (D10 ≤ 10 μm) to reduce the harmful effect of rapid water absorption. This parameter optimization maintains ease of handling while minimizing adhesion to equipment and surfaces during storage and transportation.

Inventive Principle:
Principle #35Parameter changes

3Quantity of substance

If cellulose nanofibers are dried to form a dried product, then packaging costs are reduced, but the dried product forms lumps during redispersion, reducing transfer efficiency

Engineering Contradiction:
Improvewater contentVSAvoidtransfer efficiency
Core Design Contradiction:
Quantity of substanceVSProductivity

Solution Approach 1:

The patent optimizes particle size distribution parameters (D10 ≤ 10 μm, D50 ≤ 45 μm) and water content (≤ 20% by mass) to prevent lump formation during redispersion. This ensures high transfer efficiency and productivity while maintaining cost-effectiveness through reduced packaging requirements.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The anionically modified cellulose nanofiber powder suppresses aggregation, reduces water absorption, and enhances handling and transfer efficiency while minimizing costs.

Implementation Method 1

When an aqueous dispersion of cellulose nanofibers is dried to form a dried solid, hydrogen bonds are formed between fibers of fine cellulose fibers

Methodology Applied
Scientific EffectHydrogen bonding: Chemical Bonding

Implementation Method 2

the cellulose nanofiber dried product has high hydrophilicity, and therefore the cellulose nanofibers rapidly absorb water during use and adhere to various places in a process

Methodology Applied
Scientific EffectCapillary action: Capillary Action

Data Source

PatentEP4692174A1Powder containing anionic modified cellulose nanofibers
Publication Date: 2026.02.11 NIPPON PAPER IND CO LTD
  • EP4692174A1 patent drawingFigure 1~2
  • EP4692174A1 patent drawing
  • EP4692174A1 patent drawing

AI summary

A powder containing an anionically modified cellulose nanofiber having an average fiber diameter of 3 nm to 500 nm, in which the powder has a water content of less than or equal to 20% by mass, an average particle size of less than 45 µm, and a cumulative 10% diameter (D10) of less than or equal to 10 µm in a volume-based particle diameter distribution.