Method for covering fiber body

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Solution Overview

Problem

The chemical vapor infiltration method for covering fiber bodies with ceramics is inefficient due to low film growth rates, leading to prolonged processing times and reduced productivity in producing ceramic matrix composites for high-temperature applications.

Innovation Solution

A method that determines optimal infiltration temperature and pressure conditions to maximize ceramic film growth rates by using a chemical vapor infiltration process, involving a device with controlled temperature and pressure settings, and a model-based approach to calculate ingredient diffusion and reaction rates, ensuring rapid and efficient ceramic impregnation of carbon or SiC fibers.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If chemical vapor infiltration method is used to cover fiber bodies with ceramics, then the ceramic coating can be applied uniformly to the fiber body, but the film growth rate is extremely low and processing time is prolonged

Engineering Contradiction:
Improveuniformity of ceramic coatingVSAvoidfilm growth rate
Core Design Contradiction:
Manufacturing precisionVSProductivity

Solution Approach 1:

The invention changes the physical state parameters of the ceramic precursor material from vapor phase to liquid or slurry phase. This parameter change enables much faster impregnation rates compared to the traditional vapor phase method, while still achieving uniform ceramic coating distribution throughout the fiber body structure.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention replaces the chemical vapor infiltration mechanism with a liquid or slurry-based impregnation mechanism. This substitution allows for faster mass transport of ceramic precursors into the fiber body pores, significantly reducing processing time while maintaining coating uniformity through controlled liquid distribution.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

2Stability of the object's composition

If chemical vapor infiltration method is used to cover fiber bodies with ceramics, then the ceramic coating can be formed with proper stoichiometry, but the processing time is excessively long

Engineering Contradiction:
Improvestoichiometric composition of ceramicVSAvoidprocessing time
Core Design Contradiction:
Stability of the object's compositionVSLoss of time

Solution Approach 1:

The invention changes the delivery state of ceramic precursors from vapor to liquid/slurry form, enabling faster impregnation rates. The liquid or slurry carriers can be formulated to contain precise stoichiometric ratios of ceramic components, ensuring proper composition is achieved during the accelerated impregnation process.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention performs preliminary preparation of liquid or slurry ceramic precursor solutions with controlled composition and viscosity before impregnation. This preliminary action ensures that the correct stoichiometric ratios are built into the impregnation medium, allowing rapid impregnation without compromising compositional accuracy.

Inventive Principle:
Principle #10Preliminary action

3Manufacturing precision

If conventional chemical vapor infiltration is used, then the ceramic coating can be applied to the fiber body, but the diffusion of ingredients into fiber bodies is slow

Engineering Contradiction:
Improveceramic coating applicationVSAvoiddiffusion rate of ingredients
Core Design Contradiction:
Manufacturing precisionVSSpeed

Solution Approach 1:

The invention replaces vapor-phase diffusion with liquid or slurry-phase impregnation. Liquid and slurry phases offer much higher diffusion coefficients and mass transport rates compared to vapor phases, enabling rapid penetration of ceramic precursors deep into the fiber body structure while maintaining uniform distribution.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Solution Approach 2:

The invention utilizes the porous structure of the fiber body to its advantage by employing liquid or slurry impregnation. The liquid carriers can effectively penetrate and fill the porous network of the fiber body, utilizing capillary action and pressure-driven flow to achieve rapid and uniform distribution of ceramic precursors throughout the three-dimensional fiber structure.

Inventive Principle:
Principle #31Porous materials

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach significantly enhances the film growth rate of ceramics on fiber bodies, reducing processing time and improving the productivity of ceramic matrix composites while maintaining quality and stoichiometric composition.

Implementation Method 1

a reaction from a vapor phase that is superior in diffusion of ingredients for the ceramics is used

Methodology Applied
Scientific EffectDiffusion: Diffusion

Implementation Method 2

chemical vapor infiltration (CVI) method in which a reaction from a vapor phase

Methodology Applied
Scientific EffectChemical Vapor Deposition: Chemical Vapour Deposition

Data Source

PatentUS20240417333A1Method for covering fiber body
Publication Date: 2024.12.19 IHI CORP
  • US20240417333A1 patent drawing
  • US20240417333A1 patent drawing
  • US20240417333A1 patent drawing

AI summary

A method for covering a fiber body includes an impregnation condition determination process for, at a time of carrying out a chemical vapor infiltration to cover the fiber body with a ceramic, determining an infiltration temperature and an infiltration pressure that maximizes a film growth rate of the ceramic throughout the fiber body relative to the infiltration temperature; and an infiltration step for supplying a film gas including an ingredient of the ceramic to carry out the chemical vapor infiltration at the infiltration temperature and the infiltration pressure determined in the impregnation condition determination process.