Ceramic Green Ware Body for Honeycomb Structures

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Solution Overview

Problem

The challenge lies in producing ceramic honeycomb structures with thin walls and high cell density, as existing extrusion aids often hinder economic drying and extrusion due to soluble ions, leading to inefficiencies and difficulties in achieving the desired structural properties.

Innovation Solution

A ceramic precursor batch composition with a soluble ion concentration of less than 0.75 molar, primarily composed of inorganic oxide and a temperature gelling cellulose ether, is used to facilitate extrusion and drying, eliminating soluble ions and enabling the production of honeycomb structures with thin walls and high cell density.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of manufacture

If conventional extrusion aids with soluble ions are used, then extrusion process is facilitated, but drying efficiency decreases and HSE requirements increase

Engineering Contradiction:
Improveextrusion processabilityVSAvoiddrying efficiency
Core Design Contradiction:
Ease of manufactureVSProductivity

Solution Approach 1:

The patent changes the chemical composition parameters of the extrusion aid by limiting soluble ion concentration to less than 0.75 molar and specifying particular ion ratios (Na+/K+ less than 0.1, Ca2+/Mg2+ less than 0.1). This parameter optimization enables both good extrusion processability and high drying efficiency by eliminating ions that interfere with microwave drying while maintaining workable slurry rheology.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent employs a composite extrusion aid system combining temperature-gelling cellulose ether (0.5-5 wt%) with controlled inorganic ion concentrations. This composite approach provides both the binding necessary for extrusion and the low soluble ion content required for efficient microwave drying, resolving the contradiction between manufacturability and productivity.

Inventive Principle:
Principle #40Composite materials

2Productivity

If soluble ion concentration is reduced, then drying efficiency improves, but extrusion processability may deteriorate

Engineering Contradiction:
Improvedrying efficiencyVSAvoidextrusion processability
Core Design Contradiction:
ProductivityVSEase of manufacture

Solution Approach 1:

The patent optimizes multiple parameters simultaneously: soluble ion concentration (<0.75 M), specific ion ratios (Na+/K+ <0.1, Ca2+/Mg2+ <0.1), and cellulose ether content (0.5-5 wt%). This multi-parameter optimization ensures that even with low soluble ions, the slurry maintains adequate viscosity and binding properties for extrusion while enabling rapid microwave drying.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The temperature-gelling cellulose ether acts as an intermediary substance that compensates for the reduced soluble ion content. It provides the necessary binding and rheological control for extrusion processability while not interfering with microwave drying, thus mediating between the conflicting requirements of manufacturability and drying efficiency.

Inventive Principle:
Principle #24Intermediary (Mediator)

3Manufacturing precision

If thin-walled high cell density honeycomb structures are produced, then structural performance improves, but manufacturing difficulty increases due to soluble ion interference

Engineering Contradiction:
Improvestructural propertiesVSAvoidmanufacturing difficulty
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The patent achieves thin-walled high cell density structures by optimizing extrusion parameters including soluble ion concentration (<0.75 M), cellulose ether content (0.5-5 wt%), and extrusion conditions. These parameter changes enable the formation of delicate thin walls that maintain structural integrity while achieving high cell densities (e.g., 200-400 cells per linear inch), resolving the contradiction between structural performance and manufacturing difficulty.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enhances drying efficiency and facilitates the extrusion of honeycomb structures with improved structural properties, reducing the risk of defects and lowering Health, Safety, and Environment (HSE) requirements, while allowing for microwave drying and reducing drying time by 70%.

Implementation Method 1

a temperature gelling cellulose ether

Methodology Applied
Scientific EffectTemperature gelling: Gel

Implementation Method 2

allowing for microwave drying

Methodology Applied
Scientific EffectMicrowave heating: Dielectric Heating

Data Source

PatentEP3074364B1A ceramic green ware body
Publication Date: 2020.12.23 CORNING INC
  • EP3074364B1 patent drawingFigure 1
  • EP3074364B1 patent drawingFigure 2
  • EP3074364B1 patent drawingFigure 3

AI summary

A ceramic precursor batch composition, green ware formed thereof, porous ceramic honeycomb article formed thereof, and methods of making same.