Ceramic-Metal Composite Vessels for Lithium-Ion Battery Oxide Production

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Solution Overview

Problem

Current methods for producing lithiated transition metal oxides for lithium-ion batteries face challenges such as corrosion damage in rotary kilns, slow heating and cooling rates in ceramic vessels, and high costs of ceramic matrix composites, which affect the efficiency and cycle life of the batteries.

Innovation Solution

The use of vessels comprising a ceramic matrix composite inner component and a metal or alloy outer component, allowing for faster heating and cooling rates and improved corrosion resistance, facilitating the production of oxide materials with enhanced homogeneity and reduced contamination.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If ceramic vessels are used for thermal treatment, then corrosion resistance is improved, but heating and cooling rates are limited due to thermal insulation properties

Engineering Contradiction:
Improvecorrosion resistanceVSAvoidheating and cooling rates
Core Design Contradiction:
ReliabilityVSSpeed

Solution Approach 1:

The vessel comprises an inner ceramic matrix composite component providing corrosion resistance and an outer metal component providing thermal conductivity. This composite structure combines the advantageous properties of both materials to simultaneously achieve high corrosion resistance and fast heating/cooling rates.

Inventive Principle:
Principle #40Composite materials

2Productivity

If rotary kiln is used for processing, then productivity is improved, but corrosion damage to kiln material occurs

Engineering Contradiction:
Improveprocessing efficiencyVSAvoidkiln material durability
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The processing system is segmented into removable individual vessels that can be easily exchanged, allowing continuous operation in rotary kiln while protecting the kiln material from corrosion through the corrosion-resistant vessel components.

Inventive Principle:
Principle #1Segmentation

3Speed

If entirely ceramic matrix composite vessels are used, then heating and cooling rates are improved, but manufacturing costs increase

Engineering Contradiction:
Improveheating and cooling ratesVSAvoidmanufacturing cost
Core Design Contradiction:
SpeedVSEase of manufacture

Solution Approach 1:

The vessel uses a composite structure with ceramic matrix composite inner component and metal outer component, combining the thermal performance of ceramic composites with the cost-effectiveness and thermal conductivity of metals, achieving optimal balance between performance and cost.

Inventive Principle:
Principle #40Composite materials

4Speed

If metal vessels are used, then heating and cooling rates are improved, but corrosion resistance is insufficient

Engineering Contradiction:
Improveheating and cooling ratesVSAvoidcorrosion resistance
Core Design Contradiction:
SpeedVSReliability

Solution Approach 1:

The dual-component vessel structure places the corrosion-resistant ceramic matrix composite as the inner component in direct contact with the precursor, while the metal outer component provides thermal conductivity and structural support, achieving both fast thermal response and high corrosion resistance.

Inventive Principle:
Principle #40Composite materials

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enables faster and more efficient production of oxide materials with improved homogeneity and reduced contamination, enhancing the performance and longevity of lithium-ion batteries.

Implementation Method 1

allowing for faster heating and cooling rates

Methodology Applied
Scientific EffectThermal conduction: Conduction (thermal)

Implementation Method 2

improved corrosion resistance

Methodology Applied
Scientific EffectCorrosion resistance:

Data Source

PatentEP3475247B1Open vessels and their use
Publication Date: 2021.08.11 BASF SE

AI summary

Vessels selected from crucibles, pans, open cups and saggars essentially comprising of two components, from which (A) one component being a ceramic matrix composite, and (B) the second component being from metal or alloy, and wherein component (A) is the inner one.