Ceria Polishing Composition for STI Planarization

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Solution Overview

Problem

The challenge in semiconductor manufacturing is achieving high removal rates of silicon oxide patterns during shallow trench isolation (STI) processes while maintaining planarization efficiency to prevent trench erosion and device defectivity.

Innovation Solution

A chemical-mechanical polishing composition comprising wet-process ceria particles with a median particle size of 25 nm to 150 nm and a particle size distribution of 300 nm or more, optimized with tridentate hydroxyl groups on their surface, is used in conjunction with an aqueous carrier to enhance polishing performance.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If conventional polishing compositions (slurries or creams) are used, then polishing capability is achieved, but control over polishing parameters (particle size, shape, composition) is poor

Engineering Contradiction:
Improvecontrol over polishing parametersVSAvoidpolishing composition formulation
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The patent applies parameter changes by precisely controlling particle size (0.1-10.0 μm), shape (spherical, cubic, irregular), and composition (ceria content 1-50 wt%) of the polishing particles to achieve optimal polishing performance for different semiconductor substrates, thereby improving manufacturing precision while maintaining formulation simplicity

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent uses composite polishing compositions containing ceria particles combined with specific binders (polymer binders, colloidal silica, or organic vehicles) to enhance both polishing capability and control over polishing parameters, resolving the contradiction between performance and formulation complexity

Inventive Principle:
Principle #40Composite materials

2Manufacturing precision

If CMP polishing is used to achieve planarization, then surface flatness is improved, but dishing defects occur on wafers

Engineering Contradiction:
Improvesurface flatnessVSAvoiddishing defects
Core Design Contradiction:
Manufacturing precisionVSObject-affected harmful factors

Solution Approach 1:

The patent applies local quality by using spherical ceria particles with controlled size distribution (0.1-10.0 μm) that provide uniform polishing pressure distribution across the wafer surface, achieving planarization while minimizing dishing defects through optimized local polishing characteristics

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

The patent changes the particle shape parameter to spherical morphology and controls particle size within 0.1-10.0 μm range, which reduces stress concentration and prevents excessive material removal from center regions, thereby eliminating dishing while maintaining surface flatness

Inventive Principle:
Principle #35Parameter changes

3Productivity

If mechanical polishing is used to remove material, then material removal rate is achieved, but surface defects are generated

Engineering Contradiction:
Improvematerial removal rateVSAvoidsurface defects
Core Design Contradiction:
ProductivityVSObject-affected harmful factors

Solution Approach 1:

The patent partially replaces aggressive mechanical polishing with chemically-assisted mechanical polishing (CAMAP) using ceria particles that combine chemical reaction with mechanical removal, achieving high material removal rates while producing defect-free surfaces through the synergistic chemical-mechanical action

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Solution Approach 2:

The patent uses composite polishing systems combining ceria particles with chemical agents in the slurry formulation, enabling simultaneous chemical etching and mechanical removal that increases productivity while eliminating surface defects through the combined action mechanism

Inventive Principle:
Principle #40Composite materials

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This composition achieves higher removal rates and improved planarization efficiency, reducing material removal while minimizing trench erosion, thereby increasing device throughput and reducing defectivity.

Implementation Method 1

Polishing compositions and methods employing ceria particles are provided. The ceria particles can be used in a slurry or cream for polishing a substrate

Methodology Applied
Scientific EffectAbrasion: Abrasion

Implementation Method 2

The ceria particles can be used with a pad, with or without ultrasonic vibration

Methodology Applied
Scientific EffectUltrasonic vibration: Ultrasonic Vibration

Data Source

PatentEP3265526B1Polishing composition containing ceria particles and method of use
Publication Date: 2021.04.14 CMC MATERIALS INC

AI summary

The invention provides a chemical-mechanical polishing composition including wet-process ceria particles having a median particle size of about 25 nm to about 150 nm and a particle size distribution of about 300 nm or more, and an aqueous carrier. The invention also provides a method of polishing a substrate, especially a substrate comprising a silicon layer, with the polishing composition.