Purified Chlorogenic Acid Composition via Porous Adsorbent Optimization

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Solution Overview

Problem

Existing methods for producing purified chlorogenic acid-containing compositions are limited by the caffeine-selective removing capacity of porous adsorbents, which restricts the treatable solids amount of chlorogenic acid-containing materials per unit amount of adsorbent.

Innovation Solution

A method involving a chlorogenic acid-containing composition with a solids concentration of 1.5 to 4.7 mass% and a caffeine/chlorogenic acid mass ratio of 0.001 to 2.5, contacted with a porous adsorbent at 50°C to 100°C, enhances the caffeine-selective removing property and increases the treatable solids amount.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If conventional methods use porous adsorbents to remove caffeine from chlorogenic acid-containing compositions, then caffeine removal is achieved, but the treatable solids amount per unit amount of adsorbent is limited

Engineering Contradiction:
Improvetreatable solids amountVSAvoidcaffeine removal efficiency
Core Design Contradiction:
Quantity of substanceVSProductivity

Solution Approach 1:

The patent applies parameter changes by optimizing the solids concentration of the chlorogenic acid-containing composition to a specific range (1.5-4.7 mass%) and controlling the caffeine/chlorogenic acid mass ratio (0.001-2.5). These parameter adjustments enhance the caffeine-selective removing property of the porous adsorbent, allowing increased treatable solids amount per unit amount of adsorbent while maintaining high caffeine removal efficiency.

Inventive Principle:
Principle #35Parameter changes

2Quantity of substance

If the solids concentration of chlorogenic acid-containing composition is increased, then more material can be processed, but the caffeine-selective removing capacity of the adsorbent decreases

Engineering Contradiction:
Improvesolids concentrationVSAvoidcaffeine-selective removing capacity
Core Design Contradiction:
Quantity of substanceVSReliability

Solution Approach 1:

The patent resolves this contradiction by identifying and applying optimal parameter ranges: solids concentration of 1.5-4.7 mass% and caffeine/chlorogenic acid mass ratio of 0.001-2.5. Within these parameters, the adsorbent maintains high caffeine-selective removing capacity while enabling increased solids concentration for more efficient processing.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach effectively increases the treatable solids amount of chlorogenic acid-containing material per unit of porous adsorbent while maintaining a high caffeine removal efficiency, producing a purified chlorogenic acid composition with improved yield and quality.

Implementation Method 1

When a chlorogenic acid-containing composition is brought into contact with a porous adsorbent, such as activated carbon or clay, the porous adsorbent adsorbs and removes not only caffeine

Methodology Applied
Scientific EffectAdsorption: Adsorption

Data Source

PatentEP3533334B1Refined chlorogenic acid-containing composition manufacturing method
Publication Date: 2024.09.11 KAO CORP

AI summary

Provided is a method of producing a purified chlorogenic acid-containing composition, including a contact step of bringing a chlorogenic acid-containing composition having solids concentration of from 1.5 mass% to 4.7 mass% and a "caffeine/chlorogenic acid" mass ratio of 5 or less into contact with a porous adsorbent.