Chlorogenic Acid Extraction from Coffee Beans

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

Existing methods for producing chlorogenic acid-containing compositions are complex and do not effectively prevent turbidity when the concentration of chlorogenic acid is diluted, particularly in acidic beverages.

Innovation Solution

Using specific properties of coffee beans, such as green, decaffeinated, or roasted coffee beans with certain L values, and subjecting them to column extraction with an aqueous solvent to produce a chlorogenic acid-containing composition that minimizes turbidity even at optimal concentrations.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If conventional extraction methods are used to produce chlorogenic acid-containing compositions, then the production process becomes complex involving multiple steps including adsorbent contact, precipitation, and solid-liquid separation, but the method still fails to effectively prevent turbidity when the concentration is diluted to optimal beverage levels

Engineering Contradiction:
Improveturbidity controlVSAvoidproduction process complexity
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The invention extracts and removes specific interfering substances (caffeine and other precipitable compounds) from the chlorogenic acid-containing composition through selective adsorption using activated carbon or silica gel. This extraction of harmful components prevents turbidity formation upon dilution while maintaining a relatively simple production process

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The invention controls the concentration range of chlorogenic acid (0.03-5% w/v) and pH (2-7) to specific parameters that prevent turbidity formation upon dilution. By optimizing these physical-chemical parameters, the composition maintains clarity at beverage-strength concentrations without requiring complex multi-step processing

Inventive Principle:
Principle #35Parameter changes

2Quantity of substance

If the concentration of chlorogenic acid is increased to ensure effective content in beverages, then the bioactive function is improved, but turbidity occurs particularly in acidic regions

Engineering Contradiction:
Improvechlorogenic acid concentrationVSAvoidturbidity
Core Design Contradiction:
Quantity of substanceVSObject-affected harmful factors

Solution Approach 1:

The invention utilizes the precipitable compounds (caffeine and other substances) that normally cause turbidity as indicators for selective removal. By adding activated carbon or silica gel, these harmful precipitable substances are adsorbed and removed, converting the turbidity problem into a benefit where the composition becomes stable and clear upon dilution

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

Solution Approach 2:

The invention optimizes the concentration of chlorogenic acid within specific ranges (0.03-5% w/v) and controls pH (2-7) to prevent turbidity formation. These parameter optimizations allow high effective concentrations to be maintained without the harmful turbidity effect, especially in acidic beverage conditions

Inventive Principle:
Principle #35Parameter changes

3Manufacturing precision

If multiple processing steps are implemented to reduce impurities such as caffeine, then the purity of chlorogenic acid is improved, but the production complexity and time increase

Engineering Contradiction:
ImprovepurityVSAvoidproduction time
Core Design Contradiction:
Manufacturing precisionVSLoss of time

Solution Approach 1:

The invention employs selective adsorption using activated carbon or silica gel to extract and remove caffeine and other impurities from the chlorogenic acid-containing composition. This single extraction step achieves effective purification without requiring multiple sequential processing steps, thereby reducing production time while maintaining high purity

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The invention discards the adsorbed impurities (caffeine and other precipitable substances) that are removed by activated carbon or silica gel, while recovering and retaining the chlorogenic acid in the filtrate. This selective discarding and recovering approach achieves purification efficiently in one operation rather than through multiple time-consuming steps

Inventive Principle:
Principle #34Discarding and recovering

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

A simple method to produce a chlorogenic acid-containing composition with high yield and low turbidity, suitable for acidic beverages, ensuring the aesthetic quality and effective recovery of chlorogenic acid.

Implementation Method 1

subjecting the coffee beans to column extraction with an aqueous solvent

Methodology Applied
Scientific EffectExtraction: Liquid-Liquid Extraction

Data Source

PatentEP3533345B1Chlorogenic acid-containing composition manufacturing method
Publication Date: 2021.10.20 KAO CORP
  • EP3533345B1 patent drawing
  • EP3533345B1 patent drawing

AI summary

Provided is a method of producing a chlorogenic acid-containing composition, including a step of subjecting coffee beans to column extraction using an aqueous solvent, in which the coffee beans include at least one selected from the group consisting of green coffee beans, decaffeinated green coffee beans, roasted coffee beans having an L value of 40 or more, and decaffeinated roasted coffee beans having an L value of 25 or more, and include at least one selected from the group consisting of unground coffee beans and ground coffee beans having an average particle size of 2.0 mm or more.