Chromium Target Silver Content Control for Photomask Defect Reduction

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Solution Overview

Problem

Current photomask blank preparation methods using a halftone phase shift film and chromium-containing light-shielding film result in defects due to metal impurities, particularly silver, which affect pattern accuracy and reliability during repeated exposure processes.

Innovation Solution

A method involving a metallic chromium target with minimized silver content (up to 1 ppm) is used for sputtering a chromium-containing film contiguous to a silicon-containing film or transparent substrate, ensuring reduced defect formation by controlling the silver impurity level, thereby enhancing the quality of photomask blanks and minimizing defects during pattern exposure.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If a chromium-containing light-shielding film is deposited using a conventional chromium target, then the photomask blank can be manufactured, but metal impurities (particularly silver) are introduced causing defects during repeated exposure processes

Engineering Contradiction:
Improvephotomask reliabilityVSAvoidmetal impurity defects
Core Design Contradiction:
ReliabilityVSObject-generated harmful factors

Solution Approach 1:

The invention changes the purity parameter of the chromium target material, specifying that the target must have a silver content of 1 ppm or less. This parameter change in the raw material directly prevents the introduction of harmful metal impurities that cause defects during repeated photomask exposure processes.

Inventive Principle:
Principle #35Parameter changes

2Ease of manufacture

If a chromium-containing film is deposited without controlling silver content, then manufacturing is simpler, but defects form on silicon-containing films and transparent substrates during repeated exposures

Engineering Contradiction:
Improvemanufacturing simplicityVSAvoidpattern accuracy
Core Design Contradiction:
Ease of manufactureVSManufacturing precision

Solution Approach 1:

The invention imposes a specific parameter constraint on the chromium target (silver content ≤ 1 ppm) to prevent defect formation during repeated exposures, thereby maintaining high pattern accuracy while still allowing for straightforward sputtering deposition processes.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The approach significantly reduces defect formation on silicon-containing films and transparent substrates, improving pattern accuracy and reliability during repeated exposures to ArF excimer laser radiation, ensuring higher quality photomask performance.

Implementation Method 1

depositing the chromium-containing film by sputtering the metallic chromium target

Methodology Applied
Scientific EffectSputtering: Sputtering

Data Source

PatentEP3361314B1Method for preparing photomask blank and method for preparing photomask
Publication Date: 2021.09.29 SHIN ETSU CHEMICAL CO LTD
  • EP3361314B1 patent drawingFigure 1
  • EP3361314B1 patent drawingFigure 2
  • EP3361314B1 patent drawingFigure 3

AI summary

A method for preparing a photomask blank comprising a transparent substrate and a chromium-containing film contiguous thereto involves the step of depositing the chromium-containing film by sputtering a metallic chromium target having an Ag content of up to 1 ppm. When a photomask prepared from the photomask blank is repeatedly used in patternwise exposure to ArF excimer laser radiation, the number of defects formed on the photomask is minimized.