Clastic Rock Sample Transport With Hydrofluoric Acid Spill Neutralization

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Solution Overview

Problem

Transporting clastic rock samples for palynomorph analysis is challenging due to the need for hydrofluoric acid maceration, which poses safety risks and requires extensive sample preparation time at laboratories, especially in remote locations.

Innovation Solution

An apparatus comprising a housing, reaction vessel, lid, pressure release tubing, and spill neutralization padding is used to safely transport clastic rock samples pre-treated with hydrofluoric acid, utilizing a lid to isolate the reaction vessel from the environment and a spill neutralization padding to neutralize any leaks, allowing transport via unmanned vehicles.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Loss of time

If hydrofluoric acid maceration is performed at remote well sites, then sample preparation time is reduced, but safety risks increase due to handling hazardous chemicals

Engineering Contradiction:
Improvesample preparation timeVSAvoidsafety risks from hydrofluoric acid
Core Design Contradiction:
Loss of timeVSObject-affected harmful factors

Solution Approach 1:

The reaction vessel containing hydrofluoric acid and rock sample is nested within a protective housing that includes spill containment features. The housing acts as an outer container that protects against hazards while the inner reaction vessel performs the chemical treatment, allowing field maceration without increasing external safety risks.

Inventive Principle:
Principle #7Nested doll (Nesting)

Solution Approach 2:

The spill neutralization padding surrounding the reaction vessel is designed to convert the harmful effect of potential hydrofluoric acid leaks into a beneficial neutralization reaction. The碱性 padding material reacts with spilled acid to neutralize it, transforming the hazard into a safe state while enabling field processing that reduces sample preparation time.

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

2Measurement precision

If technicians travel to remote locations for sample processing, then analysis accuracy is maintained, but travel time and cost increase

Engineering Contradiction:
Improvepalynomorph analysis accuracyVSAvoidtravel time
Core Design Contradiction:
Measurement precisionVSLoss of time

Solution Approach 1:

The apparatus enables preliminary maceration action to be performed at the remote well site before sample transport. By conducting the hydrofluoric acid treatment in the field using the portable apparatus, the sample is pre-processed closer to the source, eliminating the need for technicians to travel to remote locations while maintaining analysis accuracy through proper field containment.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The apparatus is designed to be self-contained and portable, enabling field-based sample processing without requiring external laboratory facilities or technician presence at remote sites. The integrated system performs maceration, containment, and neutralization functions autonomously, allowing accurate sample preparation to occur where the sample is collected rather than requiring technician travel.

Inventive Principle:
Principle #25Self-service

3Measurement precision

If extensive sample preparation is performed at laboratories, then analysis quality is ensured, but device complexity and operational requirements increase

Engineering Contradiction:
Improveanalysis qualityVSAvoidsample preparation system complexity
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The sample preparation system is segmented into distinct functional components: a reaction vessel for chemical treatment, a protective housing for containment, spill neutralization padding for hazard mitigation, and pressure relief mechanisms for safety. This segmentation allows the complex preparation process to be divided into manageable parts that can be performed in the field with simpler equipment rather than requiring complex centralized laboratory systems.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The apparatus integrates multiple functions into a single portable unit: the reaction vessel serves both as a reaction chamber and containment vessel, the housing provides both structural support and spill containment, and the padding serves both as cushioning and chemical neutralization medium. This multi-functionality reduces the overall complexity of the system compared to separate specialized equipment for each function.

Inventive Principle:
Principle #6Universality (Multi-functionality)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The apparatus ensures safe and efficient transport of clastic rock samples, reducing sample preparation time and eliminating the need for technicians to travel to remote locations, while enabling rapid analysis of palynomorphs.

Implementation Method 1

The spill neutralization padding is configured to react with the hydrofluoric acid in an acid-base neutralization reaction in response to coming in contact with the hydrofluoric acid

Methodology Applied
Scientific EffectAcid-base neutralization reaction: Redox Reactions

Data Source

PatentUS12385896B2Transporting clastic rock samples for palynomorph analysis
Publication Date: 2025.08.12 SAUDI ARABIAN OIL CO
  • US12385896B2 patent drawing
  • US12385896B2 patent drawing
  • US12385896B2 patent drawing

AI summary

An apparatus for transporting a clastic rock sample including a palynomorph includes a housing, a reaction vessel, multiple rods, a lid, a pressure release tubing, and a spill neutralization padding. The reaction vessel is disposed within the housing. The reaction vessel is configured to hold a specified quantity of hydrofluoric acid and the clastic rock sample. The rods extend from the housing to the reaction vessel. The lid is configured to seal against the reaction vessel to isolate an inner volume of the reaction vessel from an external environment. The pressure release tubing is configured to couple to a pressure relief valve and establish fluid communication between the annular volume and the pressure relief valve. The spill neutralization padding is configured to react with the hydrofluoric acid in an acid-base neutralization reaction in response to coming in contact with the hydrofluoric acid.