Polyurethane CMP Pad Composition for Stable Conditioning Microtexture

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Solution Overview

Problem

Conventional chemical mechanical polishing pads made from soft polyurethane materials face challenges in maintaining a favorable microtexture during conditioning due to high ductility, leading to poor groove quality and increased polishing defects, which can compromise semiconductor device functionality.

Innovation Solution

A chemical mechanical polishing pad with a polishing layer composed of a reaction product of an isocyanate terminated urethane prepolymer and a curative system, including a high molecular weight polyol curative and difunctional curative, providing a balance of properties such as Shore D hardness, elongation to break, and tensile modulus, enabling effective diamond conditioning and groove formation.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If soft polyurethane materials are used for polishing pads, then polishing rate is improved, but groove quality deteriorates due to high ductility

Engineering Contradiction:
Improvepolishing rateVSAvoidgroove quality
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

The patent modifies the polyurethane material parameters by controlling the NCO index (isocyanate to hydroxyl ratio) to be 0.8-1.2 and adjusting Shore D hardness to 40-60. This parameter optimization enables the material to achieve both high elongation (100-300%) for good groove formation and sufficient hardness for maintaining groove quality during polishing operations.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates a composite polyurethane system by reacting isocyanate-terminated urethane prepolymer with a curative system containing polyol and difunctional curative. This composite approach combines the benefits of softness and ductility from polyol with the structural integrity from difunctional curative, achieving both high polishing rate and good groove quality.

Inventive Principle:
Principle #40Composite materials

2Reliability

If softer polishing pad material is used, then polishing defects are reduced, but conditioning performance deteriorates

Engineering Contradiction:
Improvepolishing defect reductionVSAvoidconditioning performance
Core Design Contradiction:
ReliabilityVSEase of manufacture

Solution Approach 1:

The patent optimizes the Shore D hardness parameter to a specific range of 40-60, which is softer than conventional pads to reduce polishing defects like micro-scratches and chatter marks. Simultaneously, the NCO index is controlled at 0.8-1.2 to ensure the material has appropriate ductility for effective diamond conditioning, creating favorable microtexture without excessive softness that would hinder conditioning.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent introduces dynamic properties to the polishing pad material by achieving high elongation (100-300%) through controlled polyurethane formulation. This dynamic characteristic allows the material to deform and recover during conditioning, enabling diamond particles to effectively create microtexture while maintaining structural integrity during polishing.

Inventive Principle:
Principle #15Dynamics

3Productivity

If high ductility material is used, then polishing rate is improved, but microtexture maintenance deteriorates during conditioning

Engineering Contradiction:
Improvepolishing rateVSAvoidmicrotexture stability
Core Design Contradiction:
ProductivityVSStability of the object's composition

Solution Approach 1:

The patent carefully balances the Shore D hardness parameter at 40-60 and elongation at 100-300% through controlled polyurethane synthesis. This parameter optimization ensures the material has sufficient ductility to maintain high polishing rates while having enough structural stability to preserve favorable microtexture during repeated conditioning operations.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent performs preliminary optimization of the polyurethane formulation before the polishing process begins. By controlling the NCO index and curative system composition during manufacturing, the material is pre-configured with the optimal balance of ductility and stability, enabling it to maintain microtexture throughout the conditioning and polishing cycles without requiring frequent reconditioning.

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The polishing pad achieves efficient polishing with reduced defects by creating a desirable microtexture, maintaining high polishing rates while minimizing surface damage, thus ensuring the integrity of semiconductor devices.

Implementation Method 1

a polishing layer composed of a reaction product of an isocyanate terminated urethane prepolymer and a curative system, including a high molecular weight polyol curative and difunctional curative

Methodology Applied
Scientific EffectChemical Bonding: Chemical Bonding

Implementation Method 2

Pad surface 'conditioning' or 'dressing' is critical to maintain a consistent polishing surface for stable polishing performance. Over time the polishing surface of the polishing pad wears down, smoothing over the microtexture of the polishing surface—a phenomenon called 'glazing'.

Methodology Applied
Scientific EffectAbrasion: Abrasion

Implementation Method 3

The conditioning process as described cuts microscopic furrows into the pad surface, both abrading and plowing the pad material and renewing the polishing texture.

Methodology Applied
Scientific EffectWear: Wear

Implementation Method 4

a Shore D hardness of 40 to 60; an elongation to break of 125 to 300%; a tensile modulus of 100 to 300 (MPa)

Methodology Applied
Scientific EffectElasticity: Elasticity

Data Source

PatentUS12491604B2Chemical mechanical polishing pad
Publication Date: 2025.12.09 DOW GLOBAL TECHNOLOGIES LLC

AI summary

A chemical mechanical polishing pad is provided containing a polishing layer having a polishing surface, wherein the polishing layer comprises a reaction product of ingredients, including: an isocyanate terminated urethane prepolymer; and, a curative system, containing a high molecular weight polyol curative; and, a difunctional curative.